1-O-acetyl-2,3,6-tri-O-benzoyl-4-O-(2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl)-αβ-D-glucopyranose

Base Information

Chemical Name:1-O-acetyl-2,3,6-tri-O-benzoyl-4-O-(2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl)-αβ-D-glucopyranose
CAS No.:86158-36-3
Molecular Formula:C₅₆H₄₈O₁₇
Molecular Weight:992.987
Hs Code.:

Synonyms:1-O-acetyl-2,3,6-tri-O-benzoyl-4-O-(2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl)-αβ-D-glucopyranose

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Chemical Property of 1-O-acetyl-2,3,6-tri-O-benzoyl-4-O-(2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl)-αβ-D-glucopyranose

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Technology Process of 1-O-acetyl-2,3,6-tri-O-benzoyl-4-O-(2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl)-αβ-D-glucopyranose

There total 3 articles about 1-O-acetyl-2,3,6-tri-O-benzoyl-4-O-(2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl)-αβ-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 108-24-7
acetic anhydride

: 86158-35-2
methyl 2,3,6-tri-O-benzoyl-4-O-(2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl)-α-D-glucopyranoside

: 86158-36-3
1-O-acetyl-2,3,6-tri-O-benzoyl-4-O-(2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl)-αβ-D-glucopyranose

Guidance literature:: With sulfuric acid; acetic acid; Ambient temperature;

Reference yield:

: 57784-06-2,6344-46-3
methyl 2,3,6-tri-O-benzoyl-α-D-glucopyranoside

: 86158-36-3
1-O-acetyl-2,3,6-tri-O-benzoyl-4-O-(2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl)-αβ-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 74.2 percent / silver triflate, 4A molecular sieves / CH₂Cl₂ / 2 h / Ambient temperature

2: 96 percent / 4percent H₂SO₄-AcOH / Ambient temperature

With 4 A molecular sieve; sulfuric acid; silver trifluoromethanesulfonate; acetic acid; In dichloromethane;

Reference yield:

: 14218-08-7,41881-44-1,53297-33-9,60820-93-1,61198-82-1,67986-91-8,73068-86-7,131897-72-8,131897-73-9
2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl bromide

: 86158-36-3
1-O-acetyl-2,3,6-tri-O-benzoyl-4-O-(2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl)-αβ-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 74.2 percent / silver triflate, 4A molecular sieves / CH₂Cl₂ / 2 h / Ambient temperature

2: 96 percent / 4percent H₂SO₄-AcOH / Ambient temperature

With 4 A molecular sieve; sulfuric acid; silver trifluoromethanesulfonate; acetic acid; In dichloromethane;