C₅₅H₅₂N₂O₁₁S

Base Information

Chemical Name:C₅₅H₅₂N₂O₁₁S
CAS No.:1214741-42-0
Molecular Formula:C₅₅H₅₂N₂O₁₁S
Molecular Weight:949.091
Hs Code.:

C<sub>55</sub>H<sub>52</sub>N<sub>2</sub>O<sub>11</sub>S

Synonyms:C₅₅H₅₂N₂O₁₁S

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Chemical Property of C₅₅H₅₂N₂O₁₁S

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Technology Process of C₅₅H₅₂N₂O₁₁S

There total 11 articles about C₅₅H₅₂N₂O₁₁S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: C₅₅H₅₄N₂O₁₂S

: 1214741-42-0
C₅₅H₅₂N₂O₁₁S

Guidance literature:: With water; toluene-4-sulfonic acid; In toluene; at 60 ℃; for 22h; regioselective reaction;
DOI:10.1039/c0cc03676e

Reference yield:

: 1276565-06-0
(4-bromo-2-(3-(3,4,5-tris-benzyloxyphenyl)allyl)phenoxy)-tert-butyldimethylsilane

: 1214741-42-0
C₅₅H₅₂N₂O₁₁S

Guidance literature:: Multi-step reaction with 5 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium hydroxide / tetrahydrofuran; water / 4 h / Reflux

2: hydrogenchloride / methanol; water / 12 h / 60 °C

3: azodicarboxylic acid bis(2-methoxyethyl) ester; triphenylphosphine / toluene / 2 h / 0 - 20 °C / Inert atmosphere

4: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 3 h / 20 °C

5: water; toluene-4-sulfonic acid / toluene / 22 h / 60 °C

With hydrogenchloride; azodicarboxylic acid bis(2-methoxyethyl) ester; osmium(VIII) oxide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; water; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; water; acetone; toluene; 1: Suzuki-Miyaura coupling reaction / 3: Mitsunobu reaction;
DOI:10.1039/c0cc03676e

Reference yield:

: 1214741-31-7
(2-allyl-4-bromophenoxy)-tert-butyldimethylsilane

: 1214741-42-0
C₅₅H₅₂N₂O₁₁S

Guidance literature:: Multi-step reaction with 7 steps

1.1: ozone / methanol; dichloromethane / 2 h / -78 °C

1.2: 11 h / 20 °C

1.3: 24 h / 20 °C

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2.2: 2 h / 0 °C / Inert atmosphere

3.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium hydroxide / tetrahydrofuran; water / 4 h / Reflux

4.1: hydrogenchloride / methanol; water / 12 h / 60 °C

5.1: azodicarboxylic acid bis(2-methoxyethyl) ester; triphenylphosphine / toluene / 2 h / 0 - 20 °C / Inert atmosphere

6.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 3 h / 20 °C

7.1: water; toluene-4-sulfonic acid / toluene / 22 h / 60 °C

With hydrogenchloride; azodicarboxylic acid bis(2-methoxyethyl) ester; osmium(VIII) oxide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; water; toluene-4-sulfonic acid; ozone; 4-methylmorpholine N-oxide; triphenylphosphine; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; water; acetone; toluene; 2.1: Julia-Kociensky reaction / 2.2: Julia-Kociensky reaction / 3.1: Suzuki-Miyaura coupling reaction / 5.1: Mitsunobu reaction;
DOI:10.1039/c0cc03676e