1,2,4-Triazine-6(1H)-thione, 5-[(4-chlorophenyl)methyl]-3-phenyl-

Base Information

• Chemical Name: 1,2,4-Triazine-6(1H)-thione, 5-[(4-chlorophenyl)methyl]-3-phenyl-
• CAS No.: 127525-52-4
• Molecular Formula: C16H12 Cl N3 S
• Molecular Weight: 0
• Mol file: 127525-52-4.mol

Synonyms:5-(4-Chlorobenzyl)-3-phenyl-1,2,4-triazine-6(1H)-thione

Chemical Property of 1,2,4-Triazine-6(1H)-thione, 5-[(4-chlorophenyl)methyl]-3-phenyl-

Chemical Property:

• PSA: 73.66000
• LogP: 4.44540

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,2,4-Triazine-6(1H)-thione, 5-[(4-chlorophenyl)methyl]-3-phenyl-

There total 1 articles about 1,2,4-Triazine-6(1H)-thione, 5-[(4-chlorophenyl)methyl]-3-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-(4-chlorobenzyl)-3-phenyl-1,2,4-triazin-6-(1H)-one (40108-65-4) → 5-p-chlorobenzyl-3-phenyl-1,2,4-triazin-6(1H)thione (127525-52-4)

Guidance literature:

With pyridine; tetraphosphorus decasulfide;

DOI:10.1081/NCN-200051902

Reference yield: 85.0%

5-p-chlorobenzyl-3-phenyl-1,2,4-triazin-6(1H)thione (127525-52-4) + 1-bromo-1-deoxy-2,3,4,6-tetra-O-acetyl-a-D-galactopyranoside (3068-32-4) → 1-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-phenyl-5-(4-chlorobenzyl)-1,2,4-triazin-6(1H)-thione

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1081/NCN-120023275

Reference yield: 80.0%

Lawessons reagent (19172-47-5,94367-93-8) + 5-p-chlorobenzyl-3-phenyl-1,2,4-triazin-6(1H)thione (127525-52-4) → 3-p-chlorophenyl-2-p-methoxyphenyl-5-phenyl-6H-[1,2]thiaphospholo[4,5-e][1,2,4]triazine 2-sulfide

Guidance literature:

With morpholine; In toluene; for 3h; Heating;

DOI:10.1016/S0040-4020(99)00830-3

upstream raw materials:

5-(4-chlorobenzyl)-3-phenyl-1,2,4-triazin-6-(1H)-one

Downstream raw materials:

Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-[5-(4-chloro-benzyl)-3-phenyl-6-thioxo-6H-[1,2,4]triazin-1-yl]-tetrahydro-pyran-3-yl ester

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