1,3-bis<3,5-dioxo-6-(N-hydroxylamino)-2,3,4,5-tetrahydro-1,2,4-triazin-2-yl>benzene

Base Information

• Chemical Name: 1,3-bis<3,5-dioxo-6-(N-hydroxylamino)-2,3,4,5-tetrahydro-1,2,4-triazin-2-yl>benzene
• CAS No.: 161725-63-9
• Molecular Formula: C₁₄H₁₂N₁₀O₆
• Molecular Weight: 416.313

Synonyms:1,3-bis<3,5-dioxo-6-(N-hydroxylamino)-2,3,4,5-tetrahydro-1,2,4-triazin-2-yl>benzene

Chemical Property of 1,3-bis<3,5-dioxo-6-(N-hydroxylamino)-2,3,4,5-tetrahydro-1,2,4-triazin-2-yl>benzene

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Technology Process of 1,3-bis<3,5-dioxo-6-(N-hydroxylamino)-2,3,4,5-tetrahydro-1,2,4-triazin-2-yl>benzene

There total 2 articles about 1,3-bis<3,5-dioxo-6-(N-hydroxylamino)-2,3,4,5-tetrahydro-1,2,4-triazin-2-yl>benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

1,3-bis(3,5-dioxo-6-cyano-2,3,4,5-tetrahydro-1,2,4-triazin-2-yl)benzene (133568-72-6) → 1,3-bis<3,5-dioxo-6-(N-hydroxylamino)-2,3,4,5-tetrahydro-1,2,4-triazin-2-yl>benzene (161725-63-9)

Guidance literature:

With hydroxylamine hydrochloride; In ammonium hydroxide; for 240h; Ambient temperature;

DOI:10.1135/cccc19942741

Reference yield:

ethyl 3-(3,5-dioxo-6-cyano-2,3,4,5-tetrahydro-1,2,4-triazin-2-yl)-phenylhydrazonocyanoacetylcarbamate (133568-69-1) → 1,3-bis<3,5-dioxo-6-(N-hydroxylamino)-2,3,4,5-tetrahydro-1,2,4-triazin-2-yl>benzene (161725-63-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / pyridine / 24 h / Heating

2: 76 percent / NH₂OH*HCl / aq. NH₃ / 240 h / Ambient temperature

With hydroxylamine hydrochloride; In pyridine; ammonium hydroxide;

DOI:10.1135/cccc19942741

Reference yield: 76.0%

acetic anhydride (108-24-7) + 1,3-bis<3,5-dioxo-6-(N-hydroxylamino)-2,3,4,5-tetrahydro-1,2,4-triazin-2-yl>benzene (161725-63-9) → 1,3-bis<3,5-dioxo-6-(5-methyl-1,2,4-oxadiazol-3-yl)-2,3,4,5-tetrahydro-1,2,4-triazin-2-yl>benzene

Guidance literature:

In acetic acid; for 4h; Heating;

DOI:10.1135/cccc19942741

upstream raw materials:

1,3-bis(3,5-dioxo-6-cyano-2,3,4,5-tetrahydro-1,2,4-triazin-2-yl)benzene

ethyl 3-(3,5-dioxo-6-cyano-2,3,4,5-tetrahydro-1,2,4-triazin-2-yl)-phenylhydrazonocyanoacetylcarbamate

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