n-butyloxotin cyclopentanoate hexamer

Base Information

• Chemical Name: n-butyloxotin cyclopentanoate hexamer
• CAS No.: 107135-78-4
• Molecular Formula: C₆H₆*C₆₀H₁₀₈O₁₈Sn₆
• Molecular Weight: 1907.88
• Mol file: 107135-78-4.mol

Synonyms:n-butyloxotin cyclopentanoate hexamer

Chemical Property of n-butyloxotin cyclopentanoate hexamer

Chemical Property:

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Technology Process of n-butyloxotin cyclopentanoate hexamer

There total 1 articles about n-butyloxotin cyclopentanoate hexamer which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.7%

cyclopentanecarboxylic acid (3400-45-1) + n-butylstannoic acid (2273-43-0) → n-butyloxotin cyclopentanoate hexamer (107135-78-4)

Guidance literature:

With C₆H₆; In benzene; byproducts: H2O; addn. of carboxylic acid to a suspn. of n-butylstannanoic acid in C6H6,reflux for 6 h (Dean-Stark apparatus); removal of C6H6, dissoln. of solid in benzene-hexane, keeping in a refrigerator for crystn. (2 days); elem. anal.;

DOI:10.1021/ic00254a017

upstream raw materials:

cyclopentanecarboxylic acid

n-butylstannoic acid

Refernces