Technology Process of C26H33N5O6
There total 6 articles about C26H33N5O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tris(dimethylamino)sulfonium trimethylsilyldifluoride;
In
N,N-dimethyl-formamide;
at 0 - 20 ℃;
Inert atmosphere;
DOI:10.1002/anie.201008079
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dmap; triethylamine / dichloromethane / 4 h / 0 - 20 °C
2: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 1 h / -78 - 0 °C / Inert atmosphere
3: ytterbium(III) triflate / toluene / 9 h / 20 - 80 °C
4: hydrogenchloride; water / tetrahydrofuran / 14 h / 0 - 20 °C
5: tris(dimethylamino)sulfonium trimethylsilyldifluoride / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere
With
pyridine; hydrogenchloride; dmap; trifluoromethylsulfonic anhydride; tris(dimethylamino)sulfonium trimethylsilyldifluoride; water; triethylamine; ytterbium(III) triflate;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/anie.201008079
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride; water / tetrahydrofuran / 14 h / 0 - 20 °C
2: tris(dimethylamino)sulfonium trimethylsilyldifluoride / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere
With
hydrogenchloride; tris(dimethylamino)sulfonium trimethylsilyldifluoride; water;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/anie.201008079
