5-Bromo-3-methyl-3,4-dihydroquinazolin-2(1H)-one

Base Information

Chemical Name:5-Bromo-3-methyl-3,4-dihydroquinazolin-2(1H)-one
CAS No.:861106-66-3
Molecular Formula:C₉H₉BrN₂O
Molecular Weight:241.087
Hs Code.:
European Community (EC) Number:866-234-8
Mol file:861106-66-3.mol

Synonyms:5-Bromo-3-methyl-3,4-dihydroquinazolin-2(1H)-one;861106-66-3;5-bromo-3-methyl-1,4-dihydroquinazolin-2-one;5-Bromo-3,4-dihydro-3-methylquinazolin-2(1H)-one;5-bromo-3-methyl-1,2,3,4-tetrahydroquinazolin-2-one;SCHEMBL4613887;SZMUQIIVLVKCCL-UHFFFAOYSA-N;MFCD27930245;AKOS023413493;KS-9876;CS-0151112;E76706;5-bromo-3-methyl-3,4-dihydro-1H-quinazolin-2-one

Suppliers and Price of 5-Bromo-3-methyl-3,4-dihydroquinazolin-2(1H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
5-Bromo-3,4-dihydro-3-methylquinazolin-2(1H)-one
5g
$ 3083.00

Matrix Scientific
5-Bromo-3,4-dihydro-3-methylquinazolin-2(1H)-one
1g
$ 1028.00

Matrix Scientific
5-Bromo-3,4-dihydro-3-methylquinazolin-2(1H)-one
500mg
$ 600.00

Total 6 raw suppliers

Chemical Property of 5-Bromo-3-methyl-3,4-dihydroquinazolin-2(1H)-one

Chemical Property:

Storage Temp.:Sealed in dry,Room Temperature
XLogP3:1.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:239.98983
Heavy Atom Count:13
Complexity:222

Purity/Quality:

99%, ^*data from raw suppliers

5-Bromo-3,4-dihydro-3-methylquinazolin-2(1H)-one ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN1CC2=C(C=CC=C2Br)NC1=O

Technology Process of 5-Bromo-3-methyl-3,4-dihydroquinazolin-2(1H)-one

There total 5 articles about 5-Bromo-3-methyl-3,4-dihydroquinazolin-2(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 861106-65-2
3-bromo-2-((methylamino)methyl)aniline

: 530-62-1
1,1'-carbonyldiimidazole

: 861106-66-3
5-bromo-3-methyl-3,4-dihydroquinazolin-2(1H)-one

Guidance literature:: In dichloromethane; at 20 ℃; for 12h;

Reference yield: 50.0%

: 861106-65-2
3-bromo-2-((methylamino)methyl)aniline

: 32315-10-9
bis(trichloromethyl) carbonate

: 861106-66-3
5-bromo-3-methyl-3,4-dihydroquinazolin-2(1H)-one

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 58579-54-7
3-bromo-2-(bromomethyl)-1-nitrobenzene

: 861106-66-3
5-bromo-3-methyl-3,4-dihydroquinazolin-2(1H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 12 h / 20 °C

2: iron; acetic acid / 2 h / 20 °C

3: dichloromethane / 12 h / 20 °C

With iron; acetic acid; In tetrahydrofuran; dichloromethane;