(S)-methyl 2-(4-(tert-butyl)benzamido)-3-(4-(2-(4-(heptyloxy)benzoyl)hydrazine-carbonyl)phenyl)propanoate

Base Information

Chemical Name:(S)-methyl 2-(4-(tert-butyl)benzamido)-3-(4-(2-(4-(heptyloxy)benzoyl)hydrazine-carbonyl)phenyl)propanoate
CAS No.:1443791-90-9
Molecular Formula:C₃₆H₄₅N₃O₆
Molecular Weight:615.77
Hs Code.:

Synonyms:(S)-methyl 2-(4-(tert-butyl)benzamido)-3-(4-(2-(4-(heptyloxy)benzoyl)hydrazine-carbonyl)phenyl)propanoate

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Chemical Property of (S)-methyl 2-(4-(tert-butyl)benzamido)-3-(4-(2-(4-(heptyloxy)benzoyl)hydrazine-carbonyl)phenyl)propanoate

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Technology Process of (S)-methyl 2-(4-(tert-butyl)benzamido)-3-(4-(2-(4-(heptyloxy)benzoyl)hydrazine-carbonyl)phenyl)propanoate

There total 7 articles about (S)-methyl 2-(4-(tert-butyl)benzamido)-3-(4-(2-(4-(heptyloxy)benzoyl)hydrazine-carbonyl)phenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1443791-82-9
(S)-4-(2-(4-(tert-butyl)benzamido)-3-methoxy-3-oxopropyl)benzoic acid

: 64328-64-9
4-heptyloxybenzoic hydrazide

: 1443791-90-9
(S)-methyl 2-(4-(tert-butyl)benzamido)-3-(4-(2-(4-(heptyloxy)benzoyl)hydrazine-carbonyl)phenyl)propanoate

Guidance literature:: (S)-4-(2-(4-(tert-butyl)benzamido)-3-methoxy-3-oxopropyl)benzoic acid; With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at 20 ℃; for 2h;

4-heptyloxybenzoic hydrazide; In tetrahydrofuran; for 2h;

Reference yield:

: 1443791-81-8
(S)-methyl 4-(2-(4-(tert-butyl)benzamido)-3-methoxy-3-oxopropyl)benzoate

: 1443791-90-9
(S)-methyl 2-(4-(tert-butyl)benzamido)-3-(4-(2-(4-(heptyloxy)benzoyl)hydrazine-carbonyl)phenyl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hydroxide monohydrate; water / 2 h / 0 °C

1.2: pH 7

2.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 2 h / 20 °C

With 4-methyl-morpholine; lithium hydroxide monohydrate; water; isobutyl chloroformate; In tetrahydrofuran;

Reference yield:

: 15872-42-1
4-heptyloxybenzoic acid

: 1443791-90-9
(S)-methyl 2-(4-(tert-butyl)benzamido)-3-(4-(2-(4-(heptyloxy)benzoyl)hydrazine-carbonyl)phenyl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1,1'-carbonyldiimidazole; hydrazine hydrate / tetrahydrofuran / 4 h / 20 °C

2: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 2 h / 20 °C

With 4-methyl-morpholine; hydrazine hydrate; 1,1'-carbonyldiimidazole; isobutyl chloroformate; In tetrahydrofuran;