2-diazo-5-methyl-3,4,6-trinitrophenol

Base Information

• Chemical Name: 2-diazo-5-methyl-3,4,6-trinitrophenol
• CAS No.: 97564-28-8
• Molecular Formula: C₇H₃N₅O₇
• Molecular Weight: 269.13
• Mol file: 97564-28-8.mol

Synonyms:2-diazo-5-methyl-3,4,6-trinitrophenol

Chemical Property of 2-diazo-5-methyl-3,4,6-trinitrophenol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-diazo-5-methyl-3,4,6-trinitrophenol

There total 2 articles about 2-diazo-5-methyl-3,4,6-trinitrophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

4-Amino-2,3,5,6-tetranitrotoluene (84432-53-1) → 2-diazo-5-methyl-3,4,6-trinitrophenol (97564-28-8)

Guidance literature:

With nitric acid; acetic anhydride; In acetic acid; for 1h; Ambient temperature;

DOI:10.1021/jo00363a032

Reference yield:

4-amino-N,2,3,5,6-pentanitrotoluene (84432-54-2) → 2-diazo-5-methyl-3,4,6-trinitrophenol (97564-28-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 37 percent / CHCl₃ / 60 h / Heating

2: 38 percent / 90percent nitric acid, acetic anhydride / acetic acid / 1 h / Ambient temperature

With nitric acid; acetic anhydride; In chloroform; acetic acid;

DOI:10.1021/jo00363a032

upstream raw materials:

4-Amino-2,3,5,6-tetranitrotoluene

4-amino-N,2,3,5,6-pentanitrotoluene