C₃₉H₄₀N₂O₆Si

Base Information

Chemical Name:C₃₉H₄₀N₂O₆Si
CAS No.:1092803-42-3
Molecular Formula:C₃₉H₄₀N₂O₆Si
Molecular Weight:660.842
Hs Code.:

C<sub>39</sub>H<sub>40</sub>N<sub>2</sub>O<sub>6</sub>Si

Synonyms:C₃₉H₄₀N₂O₆Si

Suppliers and Price of C₃₉H₄₀N₂O₆Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₉H₄₀N₂O₆Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₉H₄₀N₂O₆Si

There total 13 articles about C₃₉H₄₀N₂O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1092804-54-0
C₄₁H₄₂N₂O₇Si

: 1092803-42-3
C₃₉H₄₀N₂O₆Si

Guidance literature:: With ammonia; In methanol; at 20 ℃; for 16h;

Reference yield:

: 1092804-53-9
C₃₉H₄₂O₇Si

: 66-22-8,144104-68-7,18324-22-6,27072-01-1,2920-92-5,51953-19-6
uracil

: 1092803-42-3
C₃₉H₄₀N₂O₆Si

Guidance literature:: C₃₉H₄₂O₇Si; uracil; With N,O-bis-(trimethylsilyl)-acetamide; In acetonitrile; Heating;

With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; Cooling with ice; Reflux;

With ammonia; In methanol; at 20 ℃; for 16h;
DOI:10.1021/ja105875e

Reference yield:

: 2595-05-3
Diacetone D-glucose

: 1092803-42-3
C₃₉H₄₀N₂O₆Si

Guidance literature:: Multi-step reaction with 16 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1.17 h / Cooling with ice

2.1: water; acetic acid / 16 h / 20 °C

3.1: sodium periodate / 1,4-dioxane; water / 1.67 h

4.1: sodium hydroxide / water; tetrahydrofuran / 72 h / 20 °C / Cooling with ice

5.1: triethylamine / dichloromethane; methanol / 18 h / 0 - 20 °C

6.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

7.1: n-butyllithium / tetrahydrofuran / 2 h / 0 °C

7.2: 16.33 h / -78 - 20 °C

8.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C

8.2: 4 h / 50 °C

9.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

9.2: 0.5 h

10.1: triphenylphosphine / dichloromethane / 0.5 h / 0 °C

10.2: 2 h / -78 °C

11.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 6 h / 20 °C

12.1: tetrahydrofuran; hexanes / 0.5 h / -78 °C

13.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 4 h / 0 - 20 °C

14.1: sulfuric acid / 0.25 h / 20 °C

15.1: N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate / acetonitrile / 2 h / Cooling with ice; Reflux

16.1: ammonia / methanol / 16 h / 20 °C

With sodium periodate; n-butyllithium; N,O-bis-(trimethylsilyl)-acetamide; oxalyl dichloride; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; ammonia; water; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; hexanes; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil; 15.1: Vorbrugen reaction;