Technology Process of C18H27NO4
There total 3 articles about C18H27NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
alpha AD-mix;
In
water; acetone;
at 0 - 4 ℃;
for 35h;
optical yield given as %de;
Inert atmosphere;
DOI:10.1039/c2ob25727k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrahydrofuran / 7 h / 0 - 20 °C / Inert atmosphere
2: pyridine; methanesulfonyl chloride / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere
3: alpha AD-mix / water; acetone / 35 h / 0 - 4 °C / Inert atmosphere
With
pyridine; alpha AD-mix; methanesulfonyl chloride;
In
tetrahydrofuran; water; acetone;
DOI:10.1039/c2ob25727k
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine; methanesulfonyl chloride / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere
2: alpha AD-mix / water; acetone / 35 h / 0 - 4 °C / Inert atmosphere
With
pyridine; alpha AD-mix; methanesulfonyl chloride;
In
tetrahydrofuran; water; acetone;
DOI:10.1039/c2ob25727k