C₅₂H₅₈N₂O₃S

Base Information

Chemical Name:C₅₂H₅₈N₂O₃S
CAS No.:1263430-78-9
Molecular Formula:C₅₂H₅₈N₂O₃S
Molecular Weight:791.11
Hs Code.:

C<sub>52</sub>H<sub>58</sub>N<sub>2</sub>O<sub>3</sub>S

Synonyms:C₅₂H₅₈N₂O₃S

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Chemical Property of C₅₂H₅₈N₂O₃S

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Technology Process of C₅₂H₅₈N₂O₃S

There total 7 articles about C₅₂H₅₈N₂O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1263430-76-7
C₄₇H₄₈N₂O₂S

: 1263430-78-9
C₅₂H₅₈N₂O₃S

Guidance literature:: C₄₇H₄₈N₂O₂S; With borane-THF; In tetrahydrofuran; at 20 ℃; for 32h;

With N,N-dimethylethylenediamine; In tetrahydrofuran; methanol; for 3h; Reflux;

di-tert-butyl dicarbonate; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 0.5h;

Reference yield:

: 1263430-76-7
C₄₇H₄₈N₂O₂S

: 1263430-78-9
C₅₂H₅₈N₂O₃S

Guidance literature:: Multi-step reaction with 2 steps

1: borane-THF / tetrahydrofuran / 32 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 20 °C

With borane-THF; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 14470-28-1
mono-4-methoxytrityl chloride

: 1263430-78-9
C₅₂H₅₈N₂O₃S

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / 2 h

2.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / dichloromethane / 0.5 h / 20 °C

3.1: borane-THF / tetrahydrofuran / 32 h / 20 °C

3.2: 3 h / Reflux

3.3: 0.5 h / 20 °C

With borane-THF; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;