(E)-5-(3-chlorophenyl)-5-(propylamino)-4-(1-(triisopropylsilyl)-1H-pyrrol-3-yl)pent-3-en-1-ol

Base Information

Chemical Name:(E)-5-(3-chlorophenyl)-5-(propylamino)-4-(1-(triisopropylsilyl)-1H-pyrrol-3-yl)pent-3-en-1-ol
CAS No.:1193433-72-5
Molecular Formula:C₂₇H₄₃ClN₂OSi
Molecular Weight:475.19
Hs Code.:

Synonyms:(E)-5-(3-chlorophenyl)-5-(propylamino)-4-(1-(triisopropylsilyl)-1H-pyrrol-3-yl)pent-3-en-1-ol

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Chemical Property of (E)-5-(3-chlorophenyl)-5-(propylamino)-4-(1-(triisopropylsilyl)-1H-pyrrol-3-yl)pent-3-en-1-ol

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Technology Process of (E)-5-(3-chlorophenyl)-5-(propylamino)-4-(1-(triisopropylsilyl)-1H-pyrrol-3-yl)pent-3-en-1-ol

There total 1 articles about (E)-5-(3-chlorophenyl)-5-(propylamino)-4-(1-(triisopropylsilyl)-1H-pyrrol-3-yl)pent-3-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: C₁₇H₂₈NOSi^(1-)*Li⁽¹⁺⁾

: 1032080-61-7
[1-(3-Chloro-phenyl)-meth-(E)-ylidene]-propyl-amine

: 1193433-72-5
(E)-5-(3-chlorophenyl)-5-(propylamino)-4-(1-(triisopropylsilyl)-1H-pyrrol-3-yl)pent-3-en-1-ol

Guidance literature:: [1-(3-Chloro-phenyl)-meth-(E)-ylidene]-propyl-amine; With titanium(IV) isopropylate; cyclopentylmagnesium chloride; In diethyl ether; at -78 - -40 ℃; for 2.5h; Inert atmosphere;

C₁₇H₂₈NOSi^(1-)*Li⁽¹⁺⁾; In diethyl ether; at -40 - 20 ℃; for 15h; Inert atmosphere;

With water; sodium hydrogencarbonate; In diethyl ether; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol902169k