4-((Z)-5-Ethoxycarbonyl-pent-1-enyl)-benzoic acid 2-methoxy-ethoxymethyl ester

Base Information

Chemical Name:4-((Z)-5-Ethoxycarbonyl-pent-1-enyl)-benzoic acid 2-methoxy-ethoxymethyl ester
CAS No.:344904-64-9
Molecular Formula:C₁₉H₂₆O₆
Molecular Weight:350.412
Hs Code.:

Synonyms:4-((Z)-5-Ethoxycarbonyl-pent-1-enyl)-benzoic acid 2-methoxy-ethoxymethyl ester

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Chemical Property of 4-((Z)-5-Ethoxycarbonyl-pent-1-enyl)-benzoic acid 2-methoxy-ethoxymethyl ester

Chemical Property:

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Technology Process of 4-((Z)-5-Ethoxycarbonyl-pent-1-enyl)-benzoic acid 2-methoxy-ethoxymethyl ester

There total 3 articles about 4-((Z)-5-Ethoxycarbonyl-pent-1-enyl)-benzoic acid 2-methoxy-ethoxymethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108545-38-6
5-hexynoic acid ethyl ester

: 344904-64-9
4-((Z)-5-Ethoxycarbonyl-pent-1-enyl)-benzoic acid 2-methoxy-ethoxymethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 76 percent / Et₃N; CuI; Pd(P(C₆H₅)2)Cl₂

2.1: H₂; pyridine / Pd/BaSO₄ / ethanol

2.2: (iPr)NEt / CH₂Cl₂

With pyridine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; hydrogen; triethylamine; Pd-BaSO₄; In ethanol; 1.1: Castro-Stephens coupling;
DOI:10.1016/S0960-894X(01)00077-4

Reference yield:

: 619-58-9
4-iodobenzoic acid

: 344904-64-9
4-((Z)-5-Ethoxycarbonyl-pent-1-enyl)-benzoic acid 2-methoxy-ethoxymethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 76 percent / Et₃N; CuI; Pd(P(C₆H₅)2)Cl₂

2.1: H₂; pyridine / Pd/BaSO₄ / ethanol

2.2: (iPr)NEt / CH₂Cl₂

With pyridine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; hydrogen; triethylamine; Pd-BaSO₄; In ethanol; 1.1: Castro-Stephens coupling;
DOI:10.1016/S0960-894X(01)00077-4

Reference yield:

: 3970-21-6
2-Methoxyethoxymethyl chloride

: 344904-62-7
4-(5-ethoxycarbonyl-pent-1-ynyl)-benzoic acid

: 344904-64-9
4-((Z)-5-Ethoxycarbonyl-pent-1-enyl)-benzoic acid 2-methoxy-ethoxymethyl ester

: 4-((E)-5-Ethoxycarbonyl-pent-1-enyl)-benzoic acid 2-methoxy-ethoxymethyl ester

Guidance literature:: 4-(5-ethoxycarbonyl-pent-1-ynyl)-benzoic acid; With pyridine; hydrogen; Pd-BaSO₄; In ethanol;

2-Methoxyethoxymethyl chloride; With (iPr)NEt; In dichloromethane;
DOI:10.1016/S0960-894X(01)00077-4