methyl 5-({[2-(ethyloxy)-2-oxoethyl]amino}carbonyl)-2,4-dihydroxy-6-oxo-1-phenyl-1,6-dihydro-3-pyridinecarboxylate

Base Information

Chemical Name:methyl 5-({[2-(ethyloxy)-2-oxoethyl]amino}carbonyl)-2,4-dihydroxy-6-oxo-1-phenyl-1,6-dihydro-3-pyridinecarboxylate
CAS No.:1202705-92-7
Molecular Formula:C₁₈H₁₈N₂O₈
Molecular Weight:390.35
Hs Code.:

Synonyms:methyl 5-({[2-(ethyloxy)-2-oxoethyl]amino}carbonyl)-2,4-dihydroxy-6-oxo-1-phenyl-1,6-dihydro-3-pyridinecarboxylate

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Chemical Property of methyl 5-({[2-(ethyloxy)-2-oxoethyl]amino}carbonyl)-2,4-dihydroxy-6-oxo-1-phenyl-1,6-dihydro-3-pyridinecarboxylate

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Technology Process of methyl 5-({[2-(ethyloxy)-2-oxoethyl]amino}carbonyl)-2,4-dihydroxy-6-oxo-1-phenyl-1,6-dihydro-3-pyridinecarboxylate

There total 1 articles about methyl 5-({[2-(ethyloxy)-2-oxoethyl]amino}carbonyl)-2,4-dihydroxy-6-oxo-1-phenyl-1,6-dihydro-3-pyridinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.7%

: 1202705-91-6
methyl 2,4-dihydroxy-6-oxo-1-phenyl-1,6-dihydro-3-pyridinecarboxylate

: 2949-22-6
Glycine ethyl ester isocyanate

: 1202705-92-7
methyl 5-({[2-(ethyloxy)-2-oxoethyl]amino}carbonyl)-2,4-dihydroxy-6-oxo-1-phenyl-1,6-dihydro-3-pyridinecarboxylate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In 1,1,2,2-tetrachloroethylene; ISOPROPYLAMIDE; at 110 ℃; for 0.5h;

Reference yield: 48.5%

: 1202705-92-7
methyl 5-({[2-(ethyloxy)-2-oxoethyl]amino}carbonyl)-2,4-dihydroxy-6-oxo-1-phenyl-1,6-dihydro-3-pyridinecarboxylate

: 108-91-8,157973-60-9
cyclohexylamine

: 1202702-85-9
N-({5-[(cyclohexylamino)carbonyl]-4,6-dihydroxy-2-oxo-1-phenyl-1,2-dihydro-3-pyridinyl}carbonyl)glycine

Guidance literature:: methyl 5-({[2-(ethyloxy)-2-oxoethyl]amino}carbonyl)-2,4-dihydroxy-6-oxo-1-phenyl-1,6-dihydro-3-pyridinecarboxylate; cyclohexylamine; In chloroform; at 150 ℃; for 0.5h; Sealed flask; Microwave irradiation;

With sodium hydroxide; In ethanol;

With hydrogenchloride; In ethanol; water; ethyl acetate;

Reference yield: 43.9%

: 1202705-92-7
methyl 5-({[2-(ethyloxy)-2-oxoethyl]amino}carbonyl)-2,4-dihydroxy-6-oxo-1-phenyl-1,6-dihydro-3-pyridinecarboxylate

: 89381-08-8
2-Cyclopropylethylamine hydrochloride

: 1202702-91-7
N-[(5-{[(2-cyclopropylethyl)amino]carbonyl}-4,6-dihydroxy-2-oxo-1-phenyl-1,2-dihydro-3-pyridinyl)carbonyl]glycine

Guidance literature:: methyl 5-({[2-(ethyloxy)-2-oxoethyl]amino}carbonyl)-2,4-dihydroxy-6-oxo-1-phenyl-1,6-dihydro-3-pyridinecarboxylate; 2-Cyclopropylethylamine hydrochloride; In chloroform; at 150 ℃; for 0.5h; Sealed flask; Microwave irradiation;

With sodium hydroxide; In ethanol;

With hydrogenchloride; In ethanol; water;