Technology Process of C20H18FN3O6
There total 6 articles about C20H18FN3O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); sodium carbonate;
In
1,2-dimethoxyethane; water;
at 90 ℃;
for 5h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C / Reflux; Inert atmosphere
1.2: 16 h / 20 °C
2.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 48 h / 20 °C
3.1: tetra-n-butylammonium dihydrogen trifluoride; potassium hydrogen bifluoride / 6 h / 120 °C
4.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / 1,4-dioxane / 16 h / Reflux; Inert atmosphere
5.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; 1,2-dimethoxyethane / 5 h / 90 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium hydrogen bifluoride; potassium acetate; sodium hydride; sodium carbonate; tetra-n-butylammonium dihydrogen trifluoride; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; chloroform; water; mineral oil;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C / Reflux; Inert atmosphere
1.2: 16 h / 20 °C
2.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 48 h / 20 °C
3.1: tetra-n-butylammonium dihydrogen trifluoride; potassium hydrogen bifluoride / 6 h / 120 °C
4.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / 1,4-dioxane / 16 h / Reflux; Inert atmosphere
5.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; 1,2-dimethoxyethane / 5 h / 90 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium hydrogen bifluoride; potassium acetate; sodium hydride; sodium carbonate; tetra-n-butylammonium dihydrogen trifluoride; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; chloroform; water; mineral oil;