3-[(methoxy)methoxy]-1-phenyl-4-[2-(trimethylsilyl)ethynyl]-2-imidazolidinone

Base Information

Chemical Name:3-[(methoxy)methoxy]-1-phenyl-4-[2-(trimethylsilyl)ethynyl]-2-imidazolidinone
CAS No.:288371-91-5
Molecular Formula:C₁₆H₂₂N₂O₃Si
Molecular Weight:318.448
Hs Code.:

Synonyms:3-[(methoxy)methoxy]-1-phenyl-4-[2-(trimethylsilyl)ethynyl]-2-imidazolidinone

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Chemical Property of 3-[(methoxy)methoxy]-1-phenyl-4-[2-(trimethylsilyl)ethynyl]-2-imidazolidinone

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Technology Process of 3-[(methoxy)methoxy]-1-phenyl-4-[2-(trimethylsilyl)ethynyl]-2-imidazolidinone

There total 4 articles about 3-[(methoxy)methoxy]-1-phenyl-4-[2-(trimethylsilyl)ethynyl]-2-imidazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 54655-07-1
lithium trimethylsilylacetylenide

: [[(methoxy)methoxyimino]ethyl]phenylcarbamic acid methyl ester

: 288371-91-5
3-[(methoxy)methoxy]-1-phenyl-4-[2-(trimethylsilyl)ethynyl]-2-imidazolidinone

Guidance literature:: In diethyl ether; at 15 - 20 ℃;
DOI:10.1016/S0040-4020(00)00306-9

Reference yield:

: 26972-56-5
2-(phenylamino)acetaldehyde dimethyl acetal

: 288371-91-5
3-[(methoxy)methoxy]-1-phenyl-4-[2-(trimethylsilyl)ethynyl]-2-imidazolidinone

Guidance literature:: Multi-step reaction with 4 steps

1: NaHCO₃ / tetrahydrofuran / 15 h / 20 °C

2: 6N HCl / 0.5 h / 55 °C

3: diethyl ether / 1 h

4: 72 percent / diethyl ether / 15 - 20 °C

With hydrogenchloride; sodium hydrogencarbonate; In tetrahydrofuran; diethyl ether; 1: Acylation / 2: Hydrolysis / 3: Condensation / 4: Addition;
DOI:10.1016/S0040-4020(00)00306-9

Reference yield:

: (2,2-dimethoxy-ethyl)-phenyl-carbamic acid methyl ester

: 288371-91-5
3-[(methoxy)methoxy]-1-phenyl-4-[2-(trimethylsilyl)ethynyl]-2-imidazolidinone

Guidance literature:: Multi-step reaction with 3 steps

1: 6N HCl / 0.5 h / 55 °C

2: diethyl ether / 1 h

3: 72 percent / diethyl ether / 15 - 20 °C

With hydrogenchloride; In diethyl ether; 1: Hydrolysis / 2: Condensation / 3: Addition;
DOI:10.1016/S0040-4020(00)00306-9