Technology Process of C57H58Cl10N8O4P6
There total 7 articles about C57H58Cl10N8O4P6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; caesium carbonate;
In
tetrahydrofuran;
at 20 ℃;
Inert atmosphere;
DOI:10.1002/chem.201202832
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine; bis(triphenylphosphine)palladium(II) dichloride; copper(l) iodide / toluene / 15 h / 40 °C / Inert atmosphere
2: tetrabutyl ammonium fluoride; triethylamine; bis(triphenylphosphine)palladium(II) dichloride; copper(l) iodide / toluene / 16 h / 40 °C / Inert atmosphere
3: sodium hydroxide / tetrahydrofuran; ethanol; water / 0.08 h / 20 °C
4: 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; caesium carbonate / tetrahydrofuran / 20 °C / Inert atmosphere
With
copper(l) iodide; 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; bis(triphenylphosphine)palladium(II) dichloride; tetrabutyl ammonium fluoride; caesium carbonate; triethylamine; sodium hydroxide;
In
tetrahydrofuran; ethanol; water; toluene;
1: |Sonogashira Cross-Coupling / 2: |Sonogashira Cross-Coupling;
DOI:10.1002/chem.201202832
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrabutyl ammonium fluoride; triethylamine; bis(triphenylphosphine)palladium(II) dichloride; copper(l) iodide / toluene / 16 h / 40 °C / Inert atmosphere
2: sodium hydroxide / tetrahydrofuran; ethanol; water / 0.08 h / 20 °C
3: 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; caesium carbonate / tetrahydrofuran / 20 °C / Inert atmosphere
With
copper(l) iodide; 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; bis(triphenylphosphine)palladium(II) dichloride; tetrabutyl ammonium fluoride; caesium carbonate; triethylamine; sodium hydroxide;
In
tetrahydrofuran; ethanol; water; toluene;
1: |Sonogashira Cross-Coupling;
DOI:10.1002/chem.201202832