3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-acetamido-3-O-benzyl-4,6-dideoxy-2-O-methyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

Base Information

Chemical Name:3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-acetamido-3-O-benzyl-4,6-dideoxy-2-O-methyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside
CAS No.:927680-54-4
Molecular Formula:C₆₇H₇₆N₂O₁₇
Molecular Weight:1181.34
Hs Code.:

3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-acetamido-3-O-benzyl-4,6-dideoxy-2-O-methyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

Synonyms:3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-acetamido-3-O-benzyl-4,6-dideoxy-2-O-methyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

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Chemical Property of 3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-acetamido-3-O-benzyl-4,6-dideoxy-2-O-methyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

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Technology Process of 3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-acetamido-3-O-benzyl-4,6-dideoxy-2-O-methyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

There total 19 articles about 3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-acetamido-3-O-benzyl-4,6-dideoxy-2-O-methyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: C₆₅H₇₄N₂O₁₆

: 108-24-7
acetic anhydride

: 927680-54-4
3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-acetamido-3-O-benzyl-4,6-dideoxy-2-O-methyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

: C₆₇H₇₆N₂O₁₇

Guidance literature:: With pyridine; dmap; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield: 66.0%

: C₆₅H₇₄N₂O₁₆

: 108-24-7
acetic anhydride

: 3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-acetamido-3-O-benzyl-4,6-dideoxy-2-O-methyl-α-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

: 927680-54-4
3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-acetamido-3-O-benzyl-4,6-dideoxy-2-O-methyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: With pyridine; dmap; at 20 ℃;
DOI:10.1002/chem.200601245

Reference yield:

: 142776-67-8
ethyl 2-O-benzoyl-4-O-benzyl-1-thio-α-L-rhamnopyranoside

: 927680-54-4
3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-acetamido-3-O-benzyl-4,6-dideoxy-2-O-methyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 8 steps

1: 72 percent / 4 Angstroem molecular sieves; N-iodosuccinimide; trifluoromethaneulfonic acid / CH₂Cl₂ / 0 °C

2: 78 percent / 4 Angstroem molecular sieves; N-iodosuccinimide; trifluoromethaneulfonic acid / CH₂Cl₂ / 0 °C

3: 93 percent / hyrazine acetate / methanol; CH₂Cl₂ / 4 h / 20 °C

4: 76 percent / 4 Angstroem molecular sieves; N-iodosuccinimide; trifluoromethaneulfonic acid / CH₂Cl₂ / 0 °C

5: 93 percent / hyrazine acetate / methanol; CH₂Cl₂ / 4 h / 20 °C

6: 51 percent / silver(I) oxide / dimethyl sulfide / tetrahydrofuran / 20 °C

7: 99 percent / 1,3-propanedithiol; triethylamine; pyridine / H₂O / 20 °C

8: 66 percent / pyridine; 4-(dimethylamino)pyridine / 20 °C

With pyridine; 1.3-propanedithiol; dmap; N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; hydrazinium monoacetate; triethylamine; silver(l) oxide; dimethylsulfide; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1002/chem.200601245