1,1-di-tert-butyl-2,5-di(2-thienyl)-3,4-diphenylsilole

Base Information

• Chemical Name: 1,1-di-tert-butyl-2,5-di(2-thienyl)-3,4-diphenylsilole
• CAS No.: 1089758-34-8
• Molecular Formula: C₃₂H₃₄S₂Si
• Molecular Weight: 510.839
• Mol file: 1089758-34-8.mol

Synonyms:1,1-di-tert-butyl-2,5-di(2-thienyl)-3,4-diphenylsilole

Chemical Property of 1,1-di-tert-butyl-2,5-di(2-thienyl)-3,4-diphenylsilole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 1,1-di-tert-butyl-2,5-di(2-thienyl)-3,4-diphenylsilole

There total 1 articles about 1,1-di-tert-butyl-2,5-di(2-thienyl)-3,4-diphenylsilole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

bis(phenylethynyl)-di-tert-butylsilane (138622-82-9) + 2-bromothiophene (1003-09-4) → 1,1-di-tert-butyl-2,5-di(2-thienyl)-3,4-diphenylsilole (1089758-34-8)

Guidance literature:

bis(phenylethynyl)-di-tert-butylsilane; With lithium 1-naphthalenide; at 20 ℃;

With zinc(II) chloride; In tetrahydrofuran; at -10 ℃;

2-bromothiophene; With bis(triphenylphosphine)palladium(II) dichloride; In tetrahydrofuran; Reflux;

DOI:10.1002/anie.200802034

upstream raw materials:

bis(phenylethynyl)-di-tert-butylsilane

2-bromothiophene