1,4-bis(2,6-dimethyl-4-bromophenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene

Base Information

Chemical Name:1,4-bis(2,6-dimethyl-4-bromophenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene
CAS No.:181709-92-2
Molecular Formula:C₂₀H₂₂Br₂N₂
Molecular Weight:450.216
Hs Code.:

Synonyms:1,4-bis(2,6-dimethyl-4-bromophenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene

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Chemical Property of 1,4-bis(2,6-dimethyl-4-bromophenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene

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Technology Process of 1,4-bis(2,6-dimethyl-4-bromophenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene

There total 1 articles about 1,4-bis(2,6-dimethyl-4-bromophenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 24596-19-8
4-bromo-2,6-dimethylphenylamine

: 431-03-8
dimethylglyoxal

: 181709-92-2
1,4-bis(2,6-dimethyl-4-bromophenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene

Guidance literature:: With formic acid; In ethanol; for 24h; Reflux;
DOI:10.1007/s11243-011-9487-x

Reference yield: 85.0%

: bis[dimethyl(μ-dimethylsulfide)platinum(II)]

: 181709-92-2
1,4-bis(2,6-dimethyl-4-bromophenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene

: 404373-47-3
Pt(CH₃)2((CH₃)2BrC₆H₂NCCH₃)2

Guidance literature:: In toluene; ligand and Pt-complex were added to flask, cooled to -78°C, evacuated, toluene was vac. transferred, warmed to room temp., stirred at room temp. for 3 nights under N2; toluene was removed in vacuo, petroleum ether was added, collected, washed with petroleum ether, dried for several h; elem. anal.;
DOI:10.1021/ja011189x

Reference yield: 53.0%

: cis-(PtPh₂(SMe₂)2)

: 181709-92-2
1,4-bis(2,6-dimethyl-4-bromophenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene

: 881910-76-5
Ph₂Pt((4-Br-2,6-Me₃C₆H₂)-N=C(Me)-C(Me)=N-(4-Br-2,6-Me₂C₆H₂))

Guidance literature:: In toluene; diimine added to soln. of Pt complex in toluene; mixt. stirred for 18 h; solvent removed (vac.); residue dissolved (CH2Cl2); filtered; pentane added; solvent decanted; dried (vac.); elem. anal.;
DOI:10.1021/ja056694z