C₁₆H₂₆OSi

Base Information

Chemical Name:C₁₆H₂₆OSi
CAS No.:1448446-15-8
Molecular Formula:C₁₆H₂₆OSi
Molecular Weight:262.467
Hs Code.:

Synonyms:C₁₆H₂₆OSi

Suppliers and Price of C₁₆H₂₆OSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₂₆OSi

Chemical Property:

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Technology Process of C₁₆H₂₆OSi

There total 8 articles about C₁₆H₂₆OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1448446-14-7
C₁₆H₂₈OSi

: 1448446-15-8
C₁₆H₂₆OSi

Guidance literature:: With oxalyl dichloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; dimethyl sulfoxide; at -78 ℃; Inert atmosphere;
DOI:10.1002/anie.201209300

Reference yield:

: 1448446-09-0
C₉H₁₂O₂

: 1448446-15-8
C₁₆H₂₆OSi

Guidance literature:: Multi-step reaction with 5 steps

1.1: diisobutylaluminium hydride / dichloromethane / 0.42 h / -78 °C / Inert atmosphere

2.1: n-butyllithium; diisopropylamine / diethyl ether; tetrahydrofuran; hexane / 0.33 h / -78 - -50 °C / Inert atmosphere

2.2: -78 - 25 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C / Inert atmosphere

3.2: -78 - 25 °C / Inert atmosphere

4.1: hydrogenchloride / tetrahydrofuran; water / 0.25 h / 25 °C / Inert atmosphere

5.1: oxalyl dichloride; N-ethyl-N,N-diisopropylamine / dichloromethane; dimethyl sulfoxide / -78 °C / Inert atmosphere

With hydrogenchloride; n-butyllithium; oxalyl dichloride; diisobutylaluminium hydride; diisopropylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1002/anie.201209300

Reference yield:

: 138124-05-7
(1S,6R)-(-)-8-Oxabicyclo<4.3.0>non-2-en-7-one

: 1448446-15-8
C₁₆H₂₆OSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 0.5 h / -78 - -30 °C / Inert atmosphere

1.2: -78 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / dichloromethane / 0.42 h / -78 °C / Inert atmosphere

3.1: n-butyllithium; diisopropylamine / diethyl ether; tetrahydrofuran; hexane / 0.33 h / -78 - -50 °C / Inert atmosphere

3.2: -78 - 25 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C / Inert atmosphere

4.2: -78 - 25 °C / Inert atmosphere

5.1: hydrogenchloride / tetrahydrofuran; water / 0.25 h / 25 °C / Inert atmosphere

6.1: oxalyl dichloride; N-ethyl-N,N-diisopropylamine / dichloromethane; dimethyl sulfoxide / -78 °C / Inert atmosphere

With hydrogenchloride; n-butyllithium; oxalyl dichloride; diisobutylaluminium hydride; diisopropylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; dimethyl sulfoxide; 1.2: |Diels-Alder Cycloaddition;
DOI:10.1002/anie.201209300