34,38-dioxo-33-(2-propenyl-1-oxy)35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.1^3,7.1^8,12.1^13,17.1^18,22.1^23,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaene

Base Information

• Chemical Name: 34,38-dioxo-33-(2-propenyl-1-oxy)35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.1^3,7.1^8,12.1^13,17.1^18,22.1^23,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaene
• CAS No.: 84379-21-5
• Molecular Formula: C₅₀H₅₄N₄O₆
• Molecular Weight: 807.002

Synonyms:34,38-dioxo-33-(2-propenyl-1-oxy)35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.1^3,7.1^8,12.1^13,17.1^18,22.1^23,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaene

Chemical Property of 34,38-dioxo-33-(2-propenyl-1-oxy)35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.1^3,7.1^8,12.1^13,17.1^18,22.1^23,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaene

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Technology Process of 34,38-dioxo-33-(2-propenyl-1-oxy)35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.1^3,7.1^8,12.1^13,17.1^18,22.1^23,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaene

There total 10 articles about 34,38-dioxo-33-(2-propenyl-1-oxy)35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.1^3,7.1^8,12.1^13,17.1^18,22.1^23,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

1-(2-propenyl-1-oxy)-2,6-bis(bromomethyl)-4-methylbenzene (84379-31-7) + 2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-bis(hexahydro-2-oxopyrimidinyl)-1,1':3',1''-terphenyl (84379-30-6) → 34,38-dioxo-33-(2-propenyl-1-oxy)35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.13,7.18,12.113,17.118,22.123,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaene (84379-21-5)

Guidance literature:

With sodium hydride; In tetrahydrofuran; -78 deg C to reflux;

DOI:10.1039/c39820001219

Reference yield:

1-(2-propenyl-1-oxy)-2,6-(dihydroxymethyl)-4-methylbenzene (7259-92-9) → 34,38-dioxo-33-(2-propenyl-1-oxy)35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.13,7.18,12.113,17.118,22.123,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaene (84379-21-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 54 percent / PBr₃

2: 41 percent / NaH / tetrahydrofuran / -78 deg C to reflux

With phosphorus tribromide; sodium hydride; In tetrahydrofuran;

DOI:10.1039/c39820001219

Reference yield:

2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-dicarboxy-5,5',5''-trimethyl-1,1':3',1''-terphenyl (84379-28-2) → 34,38-dioxo-33-(2-propenyl-1-oxy)35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.13,7.18,12.113,17.118,22.123,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaene (84379-21-5)

Guidance literature:

Multi-step reaction with 4 steps

2: base

3: 89 percent / t-BuOK / 2-methyl-propan-2-ol

4: 41 percent / NaH / tetrahydrofuran / -78 deg C to reflux

With potassium tert-butylate; sodium hydride; In tetrahydrofuran; tert-butyl alcohol;

DOI:10.1039/c39820001219

upstream raw materials:

1-(2-propenyl-1-oxy)-2,6-bis(bromomethyl)-4-methylbenzene

2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-bis(hexahydro-2-oxopyrimidinyl)-1,1':3',1''-terphenyl

2,6-bis(hydroxymethyl)-4-methylphenol

1-(2-propenyl-1-oxy)-2,6-(dihydroxymethyl)-4-methylbenzene

Downstream raw materials:

34,38-dioxo-35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.1^3,7.1^8,12.1^13,17.1^18,22.1^23,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaen-33-ol

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