1,8-bis-[phenoxy(3,5-dicarboxylic acid dimethyl ester)]-3,6-dioxo-octane

Base Information

Chemical Name:1,8-bis-[phenoxy(3,5-dicarboxylic acid dimethyl ester)]-3,6-dioxo-octane
CAS No.:22937-67-3
Molecular Formula:C₂₆H₃₀O₁₂
Molecular Weight:534.517
Hs Code.:

Synonyms:1,8-bis-[phenoxy(3,5-dicarboxylic acid dimethyl ester)]-3,6-dioxo-octane

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Chemical Property of 1,8-bis-[phenoxy(3,5-dicarboxylic acid dimethyl ester)]-3,6-dioxo-octane

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Technology Process of 1,8-bis-[phenoxy(3,5-dicarboxylic acid dimethyl ester)]-3,6-dioxo-octane

There total 1 articles about 1,8-bis-[phenoxy(3,5-dicarboxylic acid dimethyl ester)]-3,6-dioxo-octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 13036-02-7
Dimethyl 5-hydroxyisophthalate

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 22937-67-3
1,8-bis-[phenoxy(3,5-dicarboxylic acid dimethyl ester)]-3,6-dioxo-octane

Guidance literature:: With potassium carbonate; In acetonitrile; for 10h; Inert atmosphere; Reflux;
DOI:10.1021/jm200860b

Reference yield: 70.0%

: 22937-67-3
1,8-bis-[phenoxy(3,5-dicarboxylic acid dimethyl ester)]-3,6-dioxo-octane

: 200291-46-9
tri(ethylene glycol) bis(3,5-dihydroxymethyl)phenyl ether

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/jm200860b

Reference yield:

: 22937-67-3
1,8-bis-[phenoxy(3,5-dicarboxylic acid dimethyl ester)]-3,6-dioxo-octane

: 1370287-51-6
1,8-bis-[phenoxy-(3, 5-dicarbaldehyde)]-3,6-dioxo octane

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

2: silica gel; pyridinium chlorochromate / tetrahydrofuran; dichloromethane / 1 h / 20 °C

With lithium aluminium tetrahydride; silica gel; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm200860b