tert-butyl but-2-yn-1-yl(1-methyl-4-oxocyclohexa-2,5-dien-1-yl)-carbamate

Base Information

Chemical Name:tert-butyl but-2-yn-1-yl(1-methyl-4-oxocyclohexa-2,5-dien-1-yl)-carbamate
CAS No.:1448451-12-4
Molecular Formula:C₁₆H₂₁NO₃
Molecular Weight:275.348
Hs Code.:

Synonyms:tert-butyl but-2-yn-1-yl(1-methyl-4-oxocyclohexa-2,5-dien-1-yl)-carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl but-2-yn-1-yl(1-methyl-4-oxocyclohexa-2,5-dien-1-yl)-carbamate

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Technology Process of tert-butyl but-2-yn-1-yl(1-methyl-4-oxocyclohexa-2,5-dien-1-yl)-carbamate

There total 1 articles about tert-butyl but-2-yn-1-yl(1-methyl-4-oxocyclohexa-2,5-dien-1-yl)-carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 3355-28-0
1-Bromo-2-butyne

: 418809-12-8
tert-butyl (1-methyl-4-oxocyclohexa-2,5-dien-1-yl)carbamate

: 1448451-12-4
tert-butyl but-2-yn-1-yl(1-methyl-4-oxocyclohexa-2,5-dien-1-yl)-carbamate

Guidance literature:: tert-butyl (1-methyl-4-oxocyclohexa-2,5-dien-1-yl)carbamate; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; Inert atmosphere;

1-Bromo-2-butyne; In N,N-dimethyl-formamide; mineral oil; Inert atmosphere;
DOI:10.1021/ja404593c

Reference yield: 69.0%

: 1448451-12-4
tert-butyl but-2-yn-1-yl(1-methyl-4-oxocyclohexa-2,5-dien-1-yl)-carbamate

: 93877-21-5
1,4-dibenzyloxybut-2-yne

: tert-butyl 4,5-bis((benzyloxy)methyl)-3,8a-dimethyl-6-oxo-2a1,5a,6,8a-tetrahydr obenzo[cd]indole-1(2H)-carboxylate

Guidance literature:: With bis(tri-t-butylphosphine)palladium⁽⁰⁾; In toluene; at 80 ℃; for 5h; Molecular sieve; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.tet.2020.131862