(1'R,2R,3R,4R,5R)-N-butyloxycarbonyl-2-<2-acetamido-1-(benzyloxy)ethyl>-3,4-bis(benzyloxy)-5-<(benzyloxy)methyl>pyrrolidine

Base Information

Chemical Name:(1'R,2R,3R,4R,5R)-N-butyloxycarbonyl-2-<2-acetamido-1-(benzyloxy)ethyl>-3,4-bis(benzyloxy)-5-<(benzyloxy)methyl>pyrrolidine
CAS No.:231619-01-5
Molecular Formula:C₄₂H₅₀N₂O₇
Molecular Weight:694.868
Hs Code.:

Synonyms:(1'R,2R,3R,4R,5R)-N-butyloxycarbonyl-2-<2-acetamido-1-(benzyloxy)ethyl>-3,4-bis(benzyloxy)-5-<(benzyloxy)methyl>pyrrolidine

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Chemical Property of (1'R,2R,3R,4R,5R)-N-butyloxycarbonyl-2-<2-acetamido-1-(benzyloxy)ethyl>-3,4-bis(benzyloxy)-5-<(benzyloxy)methyl>pyrrolidine

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Technology Process of (1'R,2R,3R,4R,5R)-N-butyloxycarbonyl-2-<2-acetamido-1-(benzyloxy)ethyl>-3,4-bis(benzyloxy)-5-<(benzyloxy)methyl>pyrrolidine

There total 11 articles about (1'R,2R,3R,4R,5R)-N-butyloxycarbonyl-2-<2-acetamido-1-(benzyloxy)ethyl>-3,4-bis(benzyloxy)-5-<(benzyloxy)methyl>pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 108-24-7
acetic anhydride

: 231619-00-4
(1'R,2R,3R,4R,5R)-N-butyloxycarbonyl-2-<2-amino-1-(benzyloxy)ethyl>-3,4-bis(benzyloxy)-5-<(benzyloxy)methyl>pyrrolidine

: 231619-01-5
(1'R,2R,3R,4R,5R)-N-butyloxycarbonyl-2-<2-acetamido-1-(benzyloxy)ethyl>-3,4-bis(benzyloxy)-5-<(benzyloxy)methyl>pyrrolidine

Guidance literature:: With pyridine; at 20 ℃;

Reference yield: 84.0%

: 123-72-8
butyraldehyde

: 231619-00-4
(1'R,2R,3R,4R,5R)-N-butyloxycarbonyl-2-<2-amino-1-(benzyloxy)ethyl>-3,4-bis(benzyloxy)-5-<(benzyloxy)methyl>pyrrolidine

: 231619-01-5
(1'R,2R,3R,4R,5R)-N-butyloxycarbonyl-2-<2-acetamido-1-(benzyloxy)ethyl>-3,4-bis(benzyloxy)-5-<(benzyloxy)methyl>pyrrolidine

Guidance literature:: In pyridine; Ambient temperature;
DOI:10.1021/jo9902446

Reference yield:

: 231618-86-3
(1''R,2R,3R,4R,5R)-N-butyloxycarbonyl-3,4-bis(benzyloxy)-5-<(benzyloxy)methyl>-2-<1,2-dihydroxyethyl>pyrrolidine

: 231619-01-5
(1'R,2R,3R,4R,5R)-N-butyloxycarbonyl-2-<2-acetamido-1-(benzyloxy)ethyl>-3,4-bis(benzyloxy)-5-<(benzyloxy)methyl>pyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: TsCl

1.2: NaN₃

2.1: H₂ / Pd/C

2.2: pyridine

With hydrogen; p-toluenesulfonyl chloride; palladium on activated charcoal;
DOI:10.1007/s007060200018