methyl 2-(3-phenoxy-1-methyloxycarbonyl-4-oxo-2,5-cyclohexadienyl)acetate

Base Information

Chemical Name:methyl 2-(3-phenoxy-1-methyloxycarbonyl-4-oxo-2,5-cyclohexadienyl)acetate
CAS No.:358742-95-7
Molecular Formula:C₁₇H₁₆O₆
Molecular Weight:316.31
Hs Code.:

Synonyms:methyl 2-(3-phenoxy-1-methyloxycarbonyl-4-oxo-2,5-cyclohexadienyl)acetate

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Chemical Property of methyl 2-(3-phenoxy-1-methyloxycarbonyl-4-oxo-2,5-cyclohexadienyl)acetate

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Technology Process of methyl 2-(3-phenoxy-1-methyloxycarbonyl-4-oxo-2,5-cyclohexadienyl)acetate

There total 1 articles about methyl 2-(3-phenoxy-1-methyloxycarbonyl-4-oxo-2,5-cyclohexadienyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 358742-90-2
methyl 2-(3-phenoxy-1-methyloxycarbonyl-2,5-cyclohexadienyl)acetate

: 358742-95-7
methyl 2-(3-phenoxy-1-methyloxycarbonyl-4-oxo-2,5-cyclohexadienyl)acetate

Guidance literature:: With tert.-butylhydroperoxide; dipyridinium dichromate; Celite; triethylamine; In benzene; at 20 ℃; for 6h;
DOI:10.1081/SCC-100000539

Reference yield: 82.0%

: 358742-95-7
methyl 2-(3-phenoxy-1-methyloxycarbonyl-4-oxo-2,5-cyclohexadienyl)acetate

: 3-phenoxy-4-hydroxyphenylacetic acid

Guidance literature:: With sodium hydroxide; In ethanol; water; at 20 ℃; for 6h;
DOI:10.1081/SCC-100000539

Reference yield:

: 358742-95-7
methyl 2-(3-phenoxy-1-methyloxycarbonyl-4-oxo-2,5-cyclohexadienyl)acetate

: N-[3-(3,4-dimethyl-phenyl)-propyl]-2-(4-hydroxy-3-phenoxy-phenyl)-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH / methanol / 4 h / 0 - 20 °C

2: 90 percent / HOBt; DCC / acetonitrile / 0 - 20 °C

With sodium hydroxide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In methanol; acetonitrile;
DOI:10.1016/S0960-894X(02)00479-1