2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranosyl-(1->4)-1-O-acetyl-2-azido-3,6-di-O-benzyl-2-deoxy-α,β-D-glucopyranose

Base Information

Chemical Name:2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranosyl-(1->4)-1-O-acetyl-2-azido-3,6-di-O-benzyl-2-deoxy-α,β-D-glucopyranose
CAS No.:247077-88-9
Molecular Formula:C₄₉H₄₇N₃O₁₃
Molecular Weight:885.924
Hs Code.:

Synonyms:2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranosyl-(1->4)-1-O-acetyl-2-azido-3,6-di-O-benzyl-2-deoxy-α,β-D-glucopyranose

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Chemical Property of 2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranosyl-(1->4)-1-O-acetyl-2-azido-3,6-di-O-benzyl-2-deoxy-α,β-D-glucopyranose

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Technology Process of 2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranosyl-(1->4)-1-O-acetyl-2-azido-3,6-di-O-benzyl-2-deoxy-α,β-D-glucopyranose

There total 1 articles about 2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranosyl-(1->4)-1-O-acetyl-2-azido-3,6-di-O-benzyl-2-deoxy-α,β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 190367-07-8
phenyl 4,6-O-benzylidene-2,3-di-O-benzoyl-1-thio-β-D-glucopyranoside

: 1-O-acetyl-2-azido-3,6-di-O-benzyl-2-deoxy-α,β-D-glucopyranose

: 247077-88-9
2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranosyl-(1->4)-1-O-acetyl-2-azido-3,6-di-O-benzyl-2-deoxy-α,β-D-glucopyranose

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/S0968-0896(99)00106-6

Reference yield:

: 247077-88-9
2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranosyl-(1->4)-1-O-acetyl-2-azido-3,6-di-O-benzyl-2-deoxy-α,β-D-glucopyranose

: C₄₂H₄₃N₃O₁₃

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/S0968-0896(99)00106-6

Reference yield:

: 247077-88-9
2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranosyl-(1->4)-1-O-acetyl-2-azido-3,6-di-O-benzyl-2-deoxy-α,β-D-glucopyranose

: C₄₈H₅₇N₃O₁₃Si

Guidance literature:: Multi-step reaction with 2 steps

1: aqueous trifluoroacetic acid / CH₂Cl₂ / 2 h / 20 °C

2: triethylamine; 4-(dimethylamino)pyridine / CH₂Cl₂ / 2 h / 20 °C

With dmap; triethylamine; trifluoroacetic acid; In dichloromethane; 1: Hydrolysis / 2: silylation;
DOI:10.1016/S0968-0896(99)00106-6