(3,4-dimethoxy-phenyl)-{6-[(3,4-dimethoxy-phenyl)-hydroxy-methyl]-1,4-dihydro-[1,2,4,5]tetrazin-3-yl}-methanol

Base Information

Chemical Name:(3,4-dimethoxy-phenyl)-{6-[(3,4-dimethoxy-phenyl)-hydroxy-methyl]-1,4-dihydro-[1,2,4,5]tetrazin-3-yl}-methanol
CAS No.:534619-52-8
Molecular Formula:C₂₀H₂₄N₄O₆
Molecular Weight:416.434
Hs Code.:

Synonyms:(3,4-dimethoxy-phenyl)-{6-[(3,4-dimethoxy-phenyl)-hydroxy-methyl]-1,4-dihydro-[1,2,4,5]tetrazin-3-yl}-methanol

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Chemical Property of (3,4-dimethoxy-phenyl)-{6-[(3,4-dimethoxy-phenyl)-hydroxy-methyl]-1,4-dihydro-[1,2,4,5]tetrazin-3-yl}-methanol

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Technology Process of (3,4-dimethoxy-phenyl)-{6-[(3,4-dimethoxy-phenyl)-hydroxy-methyl]-1,4-dihydro-[1,2,4,5]tetrazin-3-yl}-methanol

There total 1 articles about (3,4-dimethoxy-phenyl)-{6-[(3,4-dimethoxy-phenyl)-hydroxy-methyl]-1,4-dihydro-[1,2,4,5]tetrazin-3-yl}-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109162-10-9
3,4-dimethoxymandelimidic acid ethyl ester hydrochloride

: 534619-52-8
(3,4-dimethoxy-phenyl)-{6-[(3,4-dimethoxy-phenyl)-hydroxy-methyl]-1,4-dihydro-[1,2,4,5]tetrazin-3-yl}-methanol

Guidance literature:: With hydrazine hydrate; at 0 ℃; for 3h;
DOI:10.1021/jo020713v

Reference yield:

: 534619-52-8
(3,4-dimethoxy-phenyl)-{6-[(3,4-dimethoxy-phenyl)-hydroxy-methyl]-1,4-dihydro-[1,2,4,5]tetrazin-3-yl}-methanol

: 534619-53-9
(3,4-dimethoxyphenyl)[6-[(3,4-dimethoxyphenyl)hydroxymethyl]-1,2,4,5-tetrazin-3-yl]methanol

Guidance literature:: With iron(III) chloride; In ethanol; water; at 75 ℃; for 0.5h;
DOI:10.1021/jo020713v

Reference yield:

: 534619-52-8
(3,4-dimethoxy-phenyl)-{6-[(3,4-dimethoxy-phenyl)-hydroxy-methyl]-1,4-dihydro-[1,2,4,5]tetrazin-3-yl}-methanol

: 3,6-bis(3,4-dimethoxybenzoyl)-5-(p-chlorophenyl)-1,2,4-triazine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.02 g / FeCl₃ / ethanol; H₂O / 0.5 h / 75 °C

2: 90 percent / Dess-Martin periodinane / CH₂Cl₂ / 3.5 h / 23 °C

3: 31 percent / dioxane / 17 h / 90 °C

With iron(III) chloride; Dess-Martin periodane; In 1,4-dioxane; ethanol; dichloromethane; water;
DOI:10.1021/jo020713v