1-(4-Bromophenacyl)pyrimidine-2(1H)-one

Base Information

Chemical Name:1-(4-Bromophenacyl)pyrimidine-2(1H)-one
CAS No.:519018-55-4
Molecular Formula:C₁₂H₉BrN₂O₂
Molecular Weight:293.12
Hs Code.:
DSSTox Substance ID:DTXSID401223677
Nikkaji Number:J2.422.595J

Synonyms:DTXSID401223677;AKOS011294087;519018-55-4;1-(4-Bromophenacyl)pyrimidine-2(1H)-one;1-[2-(4-Bromophenyl)-2-oxoethyl]-2(1H)-pyrimidinone

Suppliers and Price of 1-(4-Bromophenacyl)pyrimidine-2(1H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-Bromophenacyl)pyrimidine-2(1H)-one

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:291.98474
Heavy Atom Count:17
Complexity:371

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CN(C(=O)N=C1)CC(=O)C2=CC=C(C=C2)Br

Technology Process of 1-(4-Bromophenacyl)pyrimidine-2(1H)-one

There total 1 articles about 1-(4-Bromophenacyl)pyrimidine-2(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 38353-09-2,1450-92-6
2-pyrimidinone hydrochloride

: 99-73-0,132309-76-3
para-bromophenacyl bromide

: 519018-55-4
1-[2-(4-bromophenyl)-2-oxoethyl]pyrimidin-2(1H)-one

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 48h;
DOI:10.1055/s-2006-958941

Reference yield: 85.0%

: 519018-55-4
1-[2-(4-bromophenyl)-2-oxoethyl]pyrimidin-2(1H)-one

: 2-(4-bromophenyl)oxazolo[3,2-a]pyrimidinium perchlorate

Guidance literature:: 1-[2-(4-bromophenyl)-2-oxoethyl]pyrimidin-2(1H)-one; With sulfuric acid; at 20 ℃; for 5h;

With perchloric acid;
DOI:10.1055/s-2006-958941

Reference yield:

: 519018-55-4
1-[2-(4-bromophenyl)-2-oxoethyl]pyrimidin-2(1H)-one

: 6826-26-2
5-(4-bromophenyl)-1,3-oxazol-2-amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: fuming sulfuric acid / 5 h / 20 °C

1.2: 85 percent / aq. HClO₄

2.1: 96 percent / hydrazine hydrate / acetonitrile / Heating

With sulfuric acid; hydrazine hydrate; In acetonitrile;
DOI:10.1055/s-2006-958941