(2'S) 2-[(2'-benzylamino-3'-phenylpropyl)(tosyl)amino]-2-methylpropionic acid ethyl ester

Base Information

Chemical Name:(2'S) 2-[(2'-benzylamino-3'-phenylpropyl)(tosyl)amino]-2-methylpropionic acid ethyl ester
CAS No.:511286-80-9
Molecular Formula:C₂₉H₃₆N₂O₄S
Molecular Weight:508.682
Hs Code.:

Synonyms:(2'S) 2-[(2'-benzylamino-3'-phenylpropyl)(tosyl)amino]-2-methylpropionic acid ethyl ester

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Chemical Property of (2'S) 2-[(2'-benzylamino-3'-phenylpropyl)(tosyl)amino]-2-methylpropionic acid ethyl ester

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Technology Process of (2'S) 2-[(2'-benzylamino-3'-phenylpropyl)(tosyl)amino]-2-methylpropionic acid ethyl ester

There total 3 articles about (2'S) 2-[(2'-benzylamino-3'-phenylpropyl)(tosyl)amino]-2-methylpropionic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100450-53-1
ethyl 2-methyl-N-p-toluenesulfonyl alaninate

: 511286-63-8
(4S) 3,4-dibenzyl[1,2,3]oxathiazolidine-2,2-dioxide

: 511286-80-9
(2'S) 2-[(2'-benzylamino-3'-phenylpropyl)(tosyl)amino]-2-methylpropionic acid ethyl ester

Guidance literature:: ethyl 2-methyl-N-p-toluenesulfonyl alaninate; (4S) 3,4-dibenzyl[1,2,3]oxathiazolidine-2,2-dioxide; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃;

With hydrogenchloride; In N,N-dimethyl-formamide; at 20 ℃; for 4h;
DOI:10.1021/ol027418h

Reference yield:

: 42807-45-4
N-benzyl-L-phenylalaninol

: 511286-80-9
(2'S) 2-[(2'-benzylamino-3'-phenylpropyl)(tosyl)amino]-2-methylpropionic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: imidazole; triethylamine; thionyl chloride / CH₂Cl₂ / 1 h / 0 °C

2.1: 1.35 g / rithenium(III) chloride; sodium periodate / acetonitrile; H₂O / 6 h / 0 °C

3.1: sodium hydride / dimethylformamide; various solvent(s) / 20 °C

3.2: 557 mg / hydrochloric acid / dimethylformamide; various solvent(s) / 4 h / 20 °C

With 1H-imidazole; ruthenium trichloride; sodium periodate; thionyl chloride; sodium hydride; triethylamine; In dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol027418h

Reference yield:

: 511286-78-5
(S)-3,4-Dibenzyl-[1,2,3]oxathiazolidine 2-oxide

: 511286-80-9
(2'S) 2-[(2'-benzylamino-3'-phenylpropyl)(tosyl)amino]-2-methylpropionic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1.35 g / rithenium(III) chloride; sodium periodate / acetonitrile; H₂O / 6 h / 0 °C

2.1: sodium hydride / dimethylformamide; various solvent(s) / 20 °C

2.2: 557 mg / hydrochloric acid / dimethylformamide; various solvent(s) / 4 h / 20 °C

With ruthenium trichloride; sodium periodate; sodium hydride; In water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol027418h