N-(4-methylphenyl)-3-{[(4-methylphenyl)amino]methylidene}-2-phenyl-2,3-dihydro-1H-isoindol-1-imine hydrochloride

Base Information

Chemical Name:N-(4-methylphenyl)-3-{[(4-methylphenyl)amino]methylidene}-2-phenyl-2,3-dihydro-1H-isoindol-1-imine hydrochloride
CAS No.:1393881-91-8
Molecular Formula:C₂₉H₂₅N₃*ClH
Molecular Weight:451.999
Hs Code.:

Synonyms:N-(4-methylphenyl)-3-{[(4-methylphenyl)amino]methylidene}-2-phenyl-2,3-dihydro-1H-isoindol-1-imine hydrochloride

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Chemical Property of N-(4-methylphenyl)-3-{[(4-methylphenyl)amino]methylidene}-2-phenyl-2,3-dihydro-1H-isoindol-1-imine hydrochloride

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Technology Process of N-(4-methylphenyl)-3-{[(4-methylphenyl)amino]methylidene}-2-phenyl-2,3-dihydro-1H-isoindol-1-imine hydrochloride

There total 2 articles about N-(4-methylphenyl)-3-{[(4-methylphenyl)amino]methylidene}-2-phenyl-2,3-dihydro-1H-isoindol-1-imine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1393881-90-7
3-chloro-2-phenyl-2H-isoindole-1-carbaldehyde

: 106-49-0,12221-03-3
p-toluidine

: 1393881-91-8
N-(4-methylphenyl)-3-{[(4-methylphenyl)amino]methylidene}-2-phenyl-2,3-dihydro-1H-isoindol-1-imine hydrochloride

Guidance literature:: In methanol; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.tet.2012.06.014

Reference yield:

: 5388-42-1
N-phenylphthalimidine

: 1393881-91-8
N-(4-methylphenyl)-3-{[(4-methylphenyl)amino]methylidene}-2-phenyl-2,3-dihydro-1H-isoindol-1-imine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: trichlorophosphate / 0.5 h / 0 - 20 °C / Inert atmosphere

1.2: 6 h / 0 - 80 °C / Inert atmosphere

1.3: 1 h / 20 °C / Inert atmosphere

2.1: methanol / 24 h / 20 °C / Inert atmosphere

With trichlorophosphate; In methanol; 1.2: Vilsmeier-Haack reaction / 1.3: Vilsmeier-Haack reaction / 2.1: Schiff reaction;
DOI:10.1016/j.tet.2012.06.014