C₁₆H₂₀O₃

Base Information

• Chemical Name: C₁₆H₂₀O₃
• CAS No.: 1423047-24-8
• Molecular Formula: C₁₆H₂₀O₃
• Molecular Weight: 260.333
• Mol file: 1423047-24-8.mol

Synonyms:C₁₆H₂₀O₃

Chemical Property of C₁₆H₂₀O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₆H₂₀O₃

There total 3 articles about C₁₆H₂₀O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C22H34O3Si → C16H20O3 (1423047-23-7) + C16H20O3 (1423047-24-8)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 1h; Inert atmosphere;

DOI:10.1021/ol400266g

Reference yield:

methyl 4-(cyclopropylidenemethyl)benzoate (454678-84-3) → C16H20O3 (1423047-23-7) + C16H20O3 (1423047-24-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C / Inert atmosphere

2: lithium hexamethyldisilazane / toluene / -78 - 20 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; 3-chloro-benzenecarboperoxoic acid; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; toluene;

DOI:10.1021/ol400266g

Reference yield:

C12H12O3 (1423047-20-4) → C16H20O3 (1423047-23-7) + C16H20O3 (1423047-24-8)

Guidance literature:

Multi-step reaction with 2 steps

1: lithium hexamethyldisilazane / toluene / -78 - 20 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; lithium hexamethyldisilazane; In tetrahydrofuran; toluene;

DOI:10.1021/ol400266g

upstream raw materials:

methyl 4-(cyclopropylidenemethyl)benzoate

C₁₂H₁₂O₃