Technology Process of C26H36O4
There total 4 articles about C26H36O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1H-imidazole; iodine; triphenylphosphine;
In
tetrahydrofuran;
at 60 - 80 ℃;
for 1h;
DOI:10.1016/j.tet.2014.04.090
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridinium p-toluenesulfonate / methanol / 20 °C
2: triphenylphosphine; 1H-imidazole; iodine / tetrahydrofuran / 1 h / 60 - 80 °C
With
1H-imidazole; iodine; pyridinium p-toluenesulfonate; triphenylphosphine;
In
tetrahydrofuran; methanol;
DOI:10.1016/j.tet.2014.04.090
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride; tetra-(n-butyl)ammonium iodide / mineral oil; N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere
1.2: 5 h / 20 °C
2.1: pyridinium p-toluenesulfonate / methanol / 20 °C
3.1: triphenylphosphine; 1H-imidazole; iodine / tetrahydrofuran / 1 h / 60 - 80 °C
With
1H-imidazole; iodine; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; sodium hydride; triphenylphosphine;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.tet.2014.04.090