3-amino-5-tert-butoxycarbonylaminobenzoic acid 2-[2-(2-methoxyethoxy)ethoxy]ethyl ester

Base Information

Chemical Name:3-amino-5-tert-butoxycarbonylaminobenzoic acid 2-[2-(2-methoxyethoxy)ethoxy]ethyl ester
CAS No.:936353-93-4
Molecular Formula:C₁₉H₃₀N₂O₇
Molecular Weight:398.456
Hs Code.:

Synonyms:3-amino-5-tert-butoxycarbonylaminobenzoic acid 2-[2-(2-methoxyethoxy)ethoxy]ethyl ester

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Chemical Property of 3-amino-5-tert-butoxycarbonylaminobenzoic acid 2-[2-(2-methoxyethoxy)ethoxy]ethyl ester

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Technology Process of 3-amino-5-tert-butoxycarbonylaminobenzoic acid 2-[2-(2-methoxyethoxy)ethoxy]ethyl ester

There total 6 articles about 3-amino-5-tert-butoxycarbonylaminobenzoic acid 2-[2-(2-methoxyethoxy)ethoxy]ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 676999-10-3
2‐[2‐(2‐methoxyethoxy)ethoxy]ethyl 3,5‐diaminobenzoate

: 936353-93-4
3-amino-5-tert-butoxycarbonylaminobenzoic acid 2-[2-(2-methoxyethoxy)ethoxy]ethyl ester

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃;
DOI:10.1021/ja064515n

Reference yield:

: 99-33-2
3,5-dinitrobenoyl chloride

: 936353-93-4
3-amino-5-tert-butoxycarbonylaminobenzoic acid 2-[2-(2-methoxyethoxy)ethoxy]ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂ / 0 - 20 °C

2: 25 g / H₂ / Pd/C / methanol

3: 55 percent / NaOH / tetrahydrofuran; H₂O / 0 - 20 °C

With sodium hydroxide; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/ja064515n

Reference yield:

: 93310-27-1
2‐[2‐(2‐methoxyethoxy)ethoxy]ethyl 3,5‐dinitrobenzoate

: 936353-93-4
3-amino-5-tert-butoxycarbonylaminobenzoic acid 2-[2-(2-methoxyethoxy)ethoxy]ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 25 g / H₂ / Pd/C / methanol

2: 55 percent / NaOH / tetrahydrofuran; H₂O / 0 - 20 °C

With sodium hydroxide; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; water;
DOI:10.1021/ja064515n