C₅₃H₆₈N₂O₁₈S

Base Information

Chemical Name:C₅₃H₆₈N₂O₁₈S
CAS No.:869317-76-0
Molecular Formula:C₅₃H₆₈N₂O₁₈S
Molecular Weight:1053.19
Hs Code.:

C<sub>53</sub>H<sub>68</sub>N<sub>2</sub>O<sub>18</sub>S

Synonyms:C₅₃H₆₈N₂O₁₈S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₃H₆₈N₂O₁₈S

Chemical Property:

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Technology Process of C₅₃H₆₈N₂O₁₈S

There total 6 articles about C₅₃H₆₈N₂O₁₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 869317-75-9
C₅₃H₆₈N₂O₁₇S

: 869317-76-0
C₅₃H₆₈N₂O₁₈S

Guidance literature:: With ruthenium trichloride; sodium periodate; In tetrachloromethane; water; acetonitrile; at 20 ℃; for 1h;
DOI:10.1016/j.bmc.2005.06.003

Reference yield:

: 860476-67-1
carbonic acid 2-(10-allyloxyimino-14-ethyl-12,13-dihydroxy-7-methoxy-3,5,7,9,11,13-hexamethyl-2,4-dioxo-oxacyclotetradec-6-yloxy)-4-(benzyloxycarbonyl-methyl-amino)-6-methyl-tetrahydro-pyran-3-yl ester benzyl ester

: 869317-76-0
C₅₃H₆₈N₂O₁₈S

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / HCO₂H; PPh₃; Et₃N / Pd(OAc)2 / ethanol / 1 h / Heating

2: 99 percent / NaHCO₃ / dioxane / 20 °C

3: 96 percent / SOCl₂; pyridine / tetrahydrofuran / 0.5 h / 20 °C

4: 78 percent / NaIO₄; RuCl₃*nH₂O / CCl₄; acetonitrile; H₂O / 1 h / 20 °C

With pyridine; ruthenium trichloride; sodium periodate; formic acid; thionyl chloride; sodium hydrogencarbonate; triethylamine; triphenylphosphine; palladium diacetate; In tetrahydrofuran; 1,4-dioxane; tetrachloromethane; ethanol; water; acetonitrile;
DOI:10.1016/j.bmc.2005.06.003

Reference yield:

: C₅₆H₈₄N₂O₁₇

: 869317-76-0
C₅₃H₆₈N₂O₁₈S

Guidance literature:: Multi-step reaction with 6 steps

1: 99 percent / hydrochloric acid / tetrahydrofuran / 1.5 h / 20 °C

2: 85 percent / DMSO; (CF₃CO)2O; Et₃N / CH₂Cl₂ / 1 h / -78 °C

3: 76 percent / HCO₂H; PPh₃; Et₃N / Pd(OAc)2 / ethanol / 1 h / Heating

4: 99 percent / NaHCO₃ / dioxane / 20 °C

5: 96 percent / SOCl₂; pyridine / tetrahydrofuran / 0.5 h / 20 °C

6: 78 percent / NaIO₄; RuCl₃*nH₂O / CCl₄; acetonitrile; H₂O / 1 h / 20 °C

With pyridine; hydrogenchloride; ruthenium trichloride; sodium periodate; formic acid; thionyl chloride; sodium hydrogencarbonate; dimethyl sulfoxide; triethylamine; triphenylphosphine; trifluoroacetic anhydride; palladium diacetate; In tetrahydrofuran; 1,4-dioxane; tetrachloromethane; ethanol; dichloromethane; water; acetonitrile;
DOI:10.1016/j.bmc.2005.06.003