2,6-Bis(4-formylphenylcarbonyloxy)-9,10-bis[4,5-bis(methylthio)-(1,3-dithiol-2-yliden)]-9,10-dihydroanthracene

Base Information

Chemical Name:2,6-Bis(4-formylphenylcarbonyloxy)-9,10-bis[4,5-bis(methylthio)-(1,3-dithiol-2-yliden)]-9,10-dihydroanthracene
CAS No.:852996-61-3
Molecular Formula:C₄₀H₂₈O₆S₈
Molecular Weight:861.187
Hs Code.:

Synonyms:2,6-Bis(4-formylphenylcarbonyloxy)-9,10-bis[4,5-bis(methylthio)-(1,3-dithiol-2-yliden)]-9,10-dihydroanthracene

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Chemical Property of 2,6-Bis(4-formylphenylcarbonyloxy)-9,10-bis[4,5-bis(methylthio)-(1,3-dithiol-2-yliden)]-9,10-dihydroanthracene

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Technology Process of 2,6-Bis(4-formylphenylcarbonyloxy)-9,10-bis[4,5-bis(methylthio)-(1,3-dithiol-2-yliden)]-9,10-dihydroanthracene

There total 5 articles about 2,6-Bis(4-formylphenylcarbonyloxy)-9,10-bis[4,5-bis(methylthio)-(1,3-dithiol-2-yliden)]-9,10-dihydroanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 619-66-9
4-Carboxybenzaldehyde

: 159638-89-8
9,10-bis(4,5-dimethylthio-1,3-dithiol-2-ylidene)-2,6-dihydroxy-9,10-dihydroanthracene

: 852996-61-3
2,6-Bis(4-formylphenylcarbonyloxy)-9,10-bis[4,5-bis(methylthio)-(1,3-dithiol-2-yliden)]-9,10-dihydroanthracene

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 20h;
DOI:10.1002/chem.200204494

Reference yield:

: 84-60-6
anthraflavic acid

: 852996-61-3
2,6-Bis(4-formylphenylcarbonyloxy)-9,10-bis[4,5-bis(methylthio)-(1,3-dithiol-2-yliden)]-9,10-dihydroanthracene

Guidance literature:: Multi-step reaction with 4 steps

1: imidazole / dimethylformamide

2: n-BuLi / tetrahydrofuran / -78 °C

3: n-Bu₄NF / tetrahydrofuran

4: 39 percent / DCC; DMAP / CH₂Cl₂ / 20 h / 20 °C

With 1H-imidazole; dmap; n-butyllithium; tetrabutyl ammonium fluoride; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200204494

Reference yield:

: 138519-02-5
dimethyl 4,5-bis(methylthio)-1,3-dithiole phosphonate ester

: 852996-61-3
2,6-Bis(4-formylphenylcarbonyloxy)-9,10-bis[4,5-bis(methylthio)-(1,3-dithiol-2-yliden)]-9,10-dihydroanthracene

Guidance literature:: Multi-step reaction with 3 steps

1: n-BuLi / tetrahydrofuran / -78 °C

2: n-Bu₄NF / tetrahydrofuran

3: 39 percent / DCC; DMAP / CH₂Cl₂ / 20 h / 20 °C

With dmap; n-butyllithium; tetrabutyl ammonium fluoride; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.200204494