Technology Process of C13H20FISi
There total 5 articles about C13H20FISi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen fluoride;
In
tetrahydrofuran; water;
at 20 ℃;
for 1h;
DOI:10.1002/anie.201004426
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / hexanes; diethyl ether / 0.67 h / -78 °C / Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran; hexanes / -78 °C / Inert atmosphere
2.2: -78 - 30 °C / Inert atmosphere
3.1: N-iodo-succinimide; [bis(acetoxy)iodo]benzene; palladium diacetate / 1,2-dichloro-ethane / 1 h / 70 °C / Inert atmosphere
4.1: hydrogen fluoride / tetrahydrofuran; water / 1 h / 20 °C
With
N-iodo-succinimide; n-butyllithium; [bis(acetoxy)iodo]benzene; hydrogen fluoride; palladium diacetate;
In
tetrahydrofuran; hexanes; diethyl ether; water; 1,2-dichloro-ethane;
DOI:10.1002/adsc.201000975
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran; hexanes / -78 °C / Inert atmosphere
1.2: -78 - 30 °C / Inert atmosphere
2.1: N-iodo-succinimide; [bis(acetoxy)iodo]benzene; palladium diacetate / 1,2-dichloro-ethane / 1 h / 70 °C / Inert atmosphere
3.1: hydrogen fluoride / tetrahydrofuran; water / 1 h / 20 °C
With
N-iodo-succinimide; n-butyllithium; [bis(acetoxy)iodo]benzene; hydrogen fluoride; palladium diacetate;
In
tetrahydrofuran; hexanes; water; 1,2-dichloro-ethane;
DOI:10.1002/adsc.201000975
