C₅₅H₇₇N₅O₂₇S

Base Information

Chemical Name:C₅₅H₇₇N₅O₂₇S
CAS No.:676602-51-0
Molecular Formula:C₅₅H₇₇N₅O₂₇S
Molecular Weight:1272.3
Hs Code.:

C<sub>55</sub>H<sub>77</sub>N<sub>5</sub>O<sub>27</sub>S

Synonyms:C₅₅H₇₇N₅O₂₇S

Suppliers and Price of C₅₅H₇₇N₅O₂₇S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₅H₇₇N₅O₂₇S

Chemical Property:

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Technology Process of C₅₅H₇₇N₅O₂₇S

There total 5 articles about C₅₅H₇₇N₅O₂₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 60022-62-0,879278-55-4,151651-44-4
L-serine benzyl ester hydrochloride

: 676602-50-9
2-[(1-{2-(2-tert-butoxycarbonylamino-propionylamino)-3-[3,4-diacetoxy-6-acetoxymethyl-5-(3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-ylsulfanyl]-propionyl}-pyrrolidine-2-carbonyl)-amino]-3-hydroxy-propionic acid

: 676602-51-0
C₅₅H₇₇N₅O₂₇S

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;
DOI:10.1039/b311583f

Reference yield:

: 676602-42-9
C₄₀H₅₄N₄O₁₀S₂

: 676602-51-0
C₅₅H₇₇N₅O₂₇S

Guidance literature:: Multi-step reaction with 7 steps

1: aq. TFA / CH₂Cl₂

2: 68 percent / DTT; guanidinium hydrochloride / various solvent(s) / 20 °C / pH 8.0

3: 65 percent / aq. Na₂CO₃ / dimethylformamide

4: 94 percent / H₂ / Pd/C / ethyl acetate; ethanol

5: 88 percent / PyBOP; DIPEA / dimethylformamide

6: 85 percent / H₂ / Pd/C / ethyl acetate; ethanol

7: 85 percent / PyBOP; DIPEA / dimethylformamide

With DL-dithiothreitol; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; guanidine hydrochloride; sodium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium on activated charcoal; In ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1039/b311583f

Reference yield:

: 676602-48-5
1-{2-(2-tert-butoxycarbonylamino-propionylamino)-3-[3,4-diacetoxy-6-acetoxymethyl-5-(3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-ylsulfanyl]-propionyl}-pyrrolidine-2-carboxylic acid

: 676602-51-0
C₅₅H₇₇N₅O₂₇S

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / PyBOP; DIPEA / dimethylformamide

2: 85 percent / H₂ / Pd/C / ethyl acetate; ethanol

3: 85 percent / PyBOP; DIPEA / dimethylformamide

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1039/b311583f