1,3-di(2-pyridyl)benzene-5-boronic acid neopentylglycol ester

Base Information

Chemical Name:1,3-di(2-pyridyl)benzene-5-boronic acid neopentylglycol ester
CAS No.:1146691-05-5
Molecular Formula:C₂₁H₂₁BN₂O₂
Molecular Weight:344.221
Hs Code.:

Synonyms:1,3-di(2-pyridyl)benzene-5-boronic acid neopentylglycol ester

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Chemical Property of 1,3-di(2-pyridyl)benzene-5-boronic acid neopentylglycol ester

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Technology Process of 1,3-di(2-pyridyl)benzene-5-boronic acid neopentylglycol ester

There total 1 articles about 1,3-di(2-pyridyl)benzene-5-boronic acid neopentylglycol ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 150239-89-7
2,2'-(5-bromo-1,3-phenylene)dipyridine

: 201733-56-4
2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-5,5-dimethyl-1,3,2-dioxaborinane

: 1146691-05-5
1,3-di(2-pyridyl)benzene-5-boronic acid neopentylglycol ester

Guidance literature:: With KCH₃CO₂; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In dimethyl sulfoxide; (under N2); mixt. of ligand, KCH3CO2, B-compound and Pd-complex in DMSO heated at 80°C for 6 h, cooled to ambient temp., toluene added; washed with H2O, organic layer dried over K2CO3, filtered, solvent removed under reduced pressure, recrystd. from CH2Cl2-MeOH;
DOI:10.1039/b816375h

Reference yield: 78.0%

: 1146691-05-5
1,3-di(2-pyridyl)benzene-5-boronic acid neopentylglycol ester

: methyl 7-bromo-9,9-dibutyl-9H-fluorene-2-carboxylate

: C₃₉H₃₈N₂O₂

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,4-dioxane; water; for 12h; Inert atmosphere; Reflux;
DOI:10.1039/C8NJ02616E