5-oxybenzindole

Base Information

Chemical Name:5-oxybenzindole
CAS No.:14191-15-2
Molecular Formula:C₂₈H₂₃NO₃
Molecular Weight:421.496
Hs Code.:

Synonyms:5-oxybenzindole

Suppliers and Price of 5-oxybenzindole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-oxybenzindole

Chemical Property:

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Technology Process of 5-oxybenzindole

There total 1 articles about 5-oxybenzindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14191-15-2
5-oxybenzindole

Guidance literature:: Naphthochinon-(1,4), β-Benzylamino-zimtsaeure-ethylester, Eg.;
DOI:10.1039/j39670000296

Reference yield: 82.0%

: 14191-15-2
5-oxybenzindole

: 115979-13-0
ethyl ester of 1-benzyl-4,5-dioxo-2-phenylbenzindole-3-carboxylic acid

Guidance literature:: With nitric acid; In acetic acid; for 0.0833333h; Heating;
DOI:10.1007/BF00476533

Reference yield:

: 14191-15-2
5-oxybenzindole

: 115979-10-7
1-Benzyl-4-oxo-2-phenyl-1,4-dihydro-indeno[1,2-b]pyrrole-3-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / nitric acid / acetic acid / 0.08 h / Heating

2: 34 percent / 2M NaOH, 33percent H₂O₂ / methanol / 0.5 h / 20 °C

3: 58 percent / 1 h / 165 - 170 °C

4: 70 percent / trifluoroacetic anhydride / benzene / 20 °C

With sodium hydroxide; dihydrogen peroxide; nitric acid; trifluoroacetic anhydride; In methanol; acetic acid; benzene;
DOI:10.1007/BF00476533