N-[(dimethylamino)methylidene]-4-azidobenzenesulfonamide

Base Information

Chemical Name:N-[(dimethylamino)methylidene]-4-azidobenzenesulfonamide
CAS No.:1239139-81-1
Molecular Formula:C₉H₁₁N₅O₂S
Molecular Weight:253.285
Hs Code.:

Synonyms:N-[(dimethylamino)methylidene]-4-azidobenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(dimethylamino)methylidene]-4-azidobenzenesulfonamide

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Technology Process of N-[(dimethylamino)methylidene]-4-azidobenzenesulfonamide

There total 2 articles about N-[(dimethylamino)methylidene]-4-azidobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 36326-86-0
4-azidobenzenesulfonamide

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 1239139-81-1
N-[(dimethylamino)methylidene]-4-azidobenzenesulfonamide

Guidance literature:: In neat (no solvent); at 20 ℃; for 0.25h; under 760.051 Torr; Green chemistry;
DOI:10.1039/c3gc40797g

Reference yield: 73.0%

: 36326-86-0
4-azidobenzenesulfonamide

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1239139-81-1
N-[(dimethylamino)methylidene]-4-azidobenzenesulfonamide

Guidance literature:: With trichlorophosphate; at 20 ℃; for 3h;
DOI:10.1016/j.bmc.2010.05.019

Reference yield: 87.0%

: 1239139-81-1
N-[(dimethylamino)methylidene]-4-azidobenzenesulfonamide

: 117626-97-8
5'-O-(4,4'-dimethoxytrityl)-5-(1-phenyl-1H-1,2,3-triazol-4-yl)-2'-deoxyuridine

: 1239139-74-2
5-((1-(N-((dimethylamino)methylidene)aminosulfonyl)phenyl)-1,2,3-triazol-4-yl)-5'-(4,4'-dimethoxytrityl)-2'-deoxyuridine

Guidance literature:: With pyridine; copper(ll) sulfate pentahydrate; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; In tetrahydrofuran; water; tert-butyl alcohol; at 20 ℃; for 14h;
DOI:10.1016/j.bmc.2010.05.019