3-cyclohexyl-3-(dimethylphenylsilyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-propene

Base Information

Chemical Name:3-cyclohexyl-3-(dimethylphenylsilyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-propene
CAS No.:252062-23-0
Molecular Formula:C₂₃H₃₇BO₂Si
Molecular Weight:384.442
Hs Code.:

Synonyms:3-cyclohexyl-3-(dimethylphenylsilyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-propene

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Chemical Property of 3-cyclohexyl-3-(dimethylphenylsilyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-propene

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Technology Process of 3-cyclohexyl-3-(dimethylphenylsilyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-propene

There total 3 articles about 3-cyclohexyl-3-(dimethylphenylsilyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-propene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 5664-17-5
cyclohexylallene

: 185990-03-8
dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane

: 252062-23-0
3-cyclohexyl-3-(dimethylphenylsilyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-propene

Guidance literature:: With 2,6-dimethylphenyl isonitrile; In octane; a soln. of Pd(acetylacetonate)2 and isocyanide in octane was heated at 120°C for 30 s with stirring and then cooled to room temp., the borane and allene were added at room temp., the mixt. was heated at 120°C with stirring (inert atm.); bulb-to-bulb distillation; elem. anal.;
DOI:10.1016/S0022-328X(00)00472-1

Reference yield:

: 5664-17-5
cyclohexylallene

: 185990-03-8
dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane

: 252062-23-0
3-cyclohexyl-3-(dimethylphenylsilyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-propene

: (E)-1-cyclohexyl-3-(dimethylphenylsilyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-propene

Guidance literature:: With palladium(II) acetylacetonate; 1,1,3,3-tetramethylbutane isonitrile; In octane; at 120 ℃;
DOI:10.1016/S0022-328X(00)00472-1

Reference yield:

: 5664-17-5
cyclohexylallene

: 185990-03-8
dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane

: 2-{(E)-2-Cyclohexyl-1-[(dimethyl-phenyl-silanyl)-methyl]-vinyl}-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

: 252062-23-0
3-cyclohexyl-3-(dimethylphenylsilyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-propene

Guidance literature:: palladium(II) acetylacetonate; 1,1,3,3-tetramethylbutane isonitrile; In octane; at 120 ℃; for 2h; Title compound not separated from byproducts;
DOI:10.1055/s-1999-2917