tert-butyl (S)-{1-[benzhydryl(methyl)amino]-3,3-dimethyl-1-oxobutan-2-yl}carbamate

Base Information

Chemical Name:tert-butyl (S)-{1-[benzhydryl(methyl)amino]-3,3-dimethyl-1-oxobutan-2-yl}carbamate
CAS No.:1200405-67-9
Molecular Formula:C₂₅H₃₄N₂O₃
Molecular Weight:410.557
Hs Code.:

Synonyms:tert-butyl (S)-{1-[benzhydryl(methyl)amino]-3,3-dimethyl-1-oxobutan-2-yl}carbamate

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Chemical Property of tert-butyl (S)-{1-[benzhydryl(methyl)amino]-3,3-dimethyl-1-oxobutan-2-yl}carbamate

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Technology Process of tert-butyl (S)-{1-[benzhydryl(methyl)amino]-3,3-dimethyl-1-oxobutan-2-yl}carbamate

There total 1 articles about tert-butyl (S)-{1-[benzhydryl(methyl)amino]-3,3-dimethyl-1-oxobutan-2-yl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 62965-35-9
N-tert-butyloxycarbonyl-L-tert-leucine

: 14683-47-7
N-(diphenylmethyl)methylamine

: 1200405-67-9
tert-butyl (S)-{1-[benzhydryl(methyl)amino]-3,3-dimethyl-1-oxobutan-2-yl}carbamate

Guidance literature:: With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 72h; Inert atmosphere;
DOI:10.1021/ja310718f

Reference yield: 89.0%

: 1200405-67-9
tert-butyl (S)-{1-[benzhydryl(methyl)amino]-3,3-dimethyl-1-oxobutan-2-yl}carbamate

: 1186602-26-5
(S)-2-amino-N-benzhydryl-N,3,3-trimethylbutanamide

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; triethylamine; In dichloromethane; at 0 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ja310718f

Reference yield:

: 1200405-67-9
tert-butyl (S)-{1-[benzhydryl(methyl)amino]-3,3-dimethyl-1-oxobutan-2-yl}carbamate

: ethyl 1-((1R,2R)-2-(3-((S)-1-(benzhydryl(methyl)amino)-3,3-dimethyl-1-oxobutan-2-yl)thioureido)cyclohexyl)-5-methyl-2-(naphthalen-2-yl)-1H-pyrrole-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 12 h / Inert atmosphere

With triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jacs.1c10890