3H,6H-2,5-Bis-(p-N,N-dimethylaminophenyl)-1,2-thiazolino<5,4-d>1,2-thiazolin-3,6-dithion

Base Information

Chemical Name:3H,6H-2,5-Bis-(p-N,N-dimethylaminophenyl)-1,2-thiazolino<5,4-d>1,2-thiazolin-3,6-dithion
CAS No.:130626-81-2
Molecular Formula:C₂₀H₂₀N₄S₄
Molecular Weight:444.67
Hs Code.:

Synonyms:3H,6H-2,5-Bis-(p-N,N-dimethylaminophenyl)-1,2-thiazolino<5,4-d>1,2-thiazolin-3,6-dithion

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Chemical Property of 3H,6H-2,5-Bis-(p-N,N-dimethylaminophenyl)-1,2-thiazolino<5,4-d>1,2-thiazolin-3,6-dithion

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Technology Process of 3H,6H-2,5-Bis-(p-N,N-dimethylaminophenyl)-1,2-thiazolino<5,4-d>1,2-thiazolin-3,6-dithion

There total 4 articles about 3H,6H-2,5-Bis-(p-N,N-dimethylaminophenyl)-1,2-thiazolino<5,4-d>1,2-thiazolin-3,6-dithion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 56423-74-6
3H,6H-<1,2>dithiolo<4,3-c><1,2>dithiole-3,6-dithione

: 99-98-9
4-amino-N,N-dimethylaniline

: 130626-81-2
3H,6H-2,5-Bis-(p-N,N-dimethylaminophenyl)-1,2-thiazolino<5,4-d>1,2-thiazolin-3,6-dithion

Guidance literature:: In toluene; for 2.5h; Heating;

Reference yield: 32.0%

: 56423-74-6
3H,6H-<1,2>dithiolo<4,3-c><1,2>dithiole-3,6-dithione

: 99-98-9
4-amino-N,N-dimethylaniline

: 130626-82-3
3H,6H-3-(p-N,N-Dimethylaminophenyl-imino)1,2-dithiolo<4,3-c>1,2-dithiol-6-thion

: 130626-81-2
3H,6H-2,5-Bis-(p-N,N-dimethylaminophenyl)-1,2-thiazolino<5,4-d>1,2-thiazolin-3,6-dithion

Guidance literature:: In toluene;

Reference yield:

: 130626-84-5
Dikation des 3H,6H-3,6-Bis-(p-N,N-dimethylaminophenylimino)-1,2-dithiolo<4,3-c>1,2-dithiols

: 130626-81-2
3H,6H-2,5-Bis-(p-N,N-dimethylaminophenyl)-1,2-thiazolino<5,4-d>1,2-thiazolin-3,6-dithion

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / Zn / CHCl₃ / 2 h / Heating

2: 1.) HCl (gas) 2.) tetrabutylammonium iodide / 1.) chloroform 2.) chloroform, 1 h, room temperature

With hydrogenchloride; tetra-(n-butyl)ammonium iodide; zinc; In chloroform;