Technology Process of C37H53N7O11
There total 1 articles about C37H53N7O11 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
N,N'-di-[(phenylmethoxy)carbonyl]-L-lysine;
With
O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
for 0.0833333h;
Inert atmosphere;
C15H29N5O6;
In
dichloromethane;
at 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1002/asia.201000700
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 20% palladium hydroxide on charcoal; hydrogen / methanol / 3 h / 20 °C / Inert atmosphere
2: dmap / dichloromethane / 3.17 h / 0 - 20 °C / Inert atmosphere
3: water; sodium hydroxide / ethanol / 2 h / 20 °C / Inert atmosphere
4: hydrogenchloride; water / 3 h / 20 °C / Inert atmosphere
5: dimethyl sulfoxide / 1 h / 60 °C / Inert atmosphere
With
hydrogenchloride; dmap; 20% palladium hydroxide on charcoal; water; hydrogen; sodium hydroxide;
In
methanol; ethanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1002/asia.201000700