2,4,6-triiodo-5-(3-aza-5-methyl-1,4-dioxopentan-1,5-diyl-{10-[1,4,7,10-tetraazacyclododecanyl]})methylaminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentan-1,5-diyl-{10-[1,4,7,10-tetraazacyclododecanyl]})amide

Base Information

Chemical Name:2,4,6-triiodo-5-(3-aza-5-methyl-1,4-dioxopentan-1,5-diyl-{10-[1,4,7,10-tetraazacyclododecanyl]})methylaminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentan-1,5-diyl-{10-[1,4,7,10-tetraazacyclododecanyl]})amide
CAS No.:870475-47-1
Molecular Formula:C₄₈H₈₇I₃N₁₈O₆
Molecular Weight:1393.05
Hs Code.:

2,4,6-triiodo-5-(3-aza-5-methyl-1,4-dioxopentan-1,5-diyl-{10-[1,4,7,10-tetraazacyclododecanyl]})methylaminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentan-1,5-diyl-{10-[1,4,7,10-tetraazacyclododecanyl]})amide

Synonyms:2,4,6-triiodo-5-(3-aza-5-methyl-1,4-dioxopentan-1,5-diyl-{10-[1,4,7,10-tetraazacyclododecanyl]})methylaminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentan-1,5-diyl-{10-[1,4,7,10-tetraazacyclododecanyl]})amide

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Chemical Property of 2,4,6-triiodo-5-(3-aza-5-methyl-1,4-dioxopentan-1,5-diyl-{10-[1,4,7,10-tetraazacyclododecanyl]})methylaminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentan-1,5-diyl-{10-[1,4,7,10-tetraazacyclododecanyl]})amide

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Technology Process of 2,4,6-triiodo-5-(3-aza-5-methyl-1,4-dioxopentan-1,5-diyl-{10-[1,4,7,10-tetraazacyclododecanyl]})methylaminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentan-1,5-diyl-{10-[1,4,7,10-tetraazacyclododecanyl]})amide

There total 1 articles about 2,4,6-triiodo-5-(3-aza-5-methyl-1,4-dioxopentan-1,5-diyl-{10-[1,4,7,10-tetraazacyclododecanyl]})methylaminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentan-1,5-diyl-{10-[1,4,7,10-tetraazacyclododecanyl]})amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 870475-46-0
2,4,6-triiodo-5-(3-aza-5-methyl-1,4-dioxopentan-1,5-diyl-{10-[1,4,7-tris(benzyloxycarbonyl)-1,4,7,10-tetraazacyclododecanyl]})methylaminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentan-1,5-diyl-{10-[1,4,7-tris-(benzyloxycarbonyl)-1,4,7,10-tetraazacyclododecanyl]})amide

: 870475-47-1
2,4,6-triiodo-5-(3-aza-5-methyl-1,4-dioxopentan-1,5-diyl-{10-[1,4,7,10-tetraazacyclododecanyl]})methylaminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentan-1,5-diyl-{10-[1,4,7,10-tetraazacyclododecanyl]})amide

Guidance literature:: 2,4,6-triiodo-5-(3-aza-5-methyl-1,4-dioxopentan-1,5-diyl-{10-[1,4,7-tris(benzyloxycarbonyl)-1,4,7,10-tetraazacyclododecanyl]})methylaminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentan-1,5-diyl-{10-[1,4,7-tris-(benzyloxycarbonyl)-1,4,7,10-tetraazacyclododecanyl]})amide; With hydrogen bromide; acetic acid; at 0 - 20 ℃; for 3h;

With sodium hydroxide; In dichloromethane; water; pH=10;

Reference yield: 69.0%

: 870475-47-1
2,4,6-triiodo-5-(3-aza-5-methyl-1,4-dioxopentan-1,5-diyl-{10-[1,4,7,10-tetraazacyclododecanyl]})methylaminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentan-1,5-diyl-{10-[1,4,7,10-tetraazacyclododecanyl]})amide

: 79-11-8
chloroacetic acid

: 870475-48-2
2,4,6-triiodo-5-(3-aza-5-methyl-1,4-dioxopentan-1,5-diyl-{10-[1,4,7-tris(carboxymethyl)-1,4,7,10-tetraazacyclododecanyl]})methylaminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentan-1,5-diyl-{10-[1,4,7-tris-(carboxymethyl)-1,4,7,10-tetraazacyclododecanyl]})amide

Guidance literature:: 2,4,6-triiodo-5-(3-aza-5-methyl-1,4-dioxopentan-1,5-diyl-{10-[1,4,7,10-tetraazacyclododecanyl]})methylaminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentan-1,5-diyl-{10-[1,4,7,10-tetraazacyclododecanyl]})amide; chloroacetic acid; With sodium hydroxide; In water; at 70 ℃; for 10h; pH=9.5;

With hydrogenchloride; water; at 20 ℃; pH=1;