C₃₈H₅₅NO₁₀Se

Base Information

Chemical Name:C₃₈H₅₅NO₁₀Se
CAS No.:1033588-21-4
Molecular Formula:C₃₈H₅₅NO₁₀Se
Molecular Weight:764.815
Hs Code.:

C<sub>38</sub>H<sub>55</sub>NO<sub>10</sub>Se

Synonyms:C₃₈H₅₅NO₁₀Se

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Chemical Property of C₃₈H₅₅NO₁₀Se

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Technology Process of C₃₈H₅₅NO₁₀Se

There total 39 articles about C₃₈H₅₅NO₁₀Se which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1033588-18-9
C₅₆H₁₀₈O₉Si₄

: 1033588-21-4
C₃₈H₅₅NO₁₀Se

Guidance literature:: With tris(dimethylamino)sulfonium trimethylsilyldifluoride; In tetrahydrofuran; water; N,N-dimethyl-formamide; at 0 - 20 ℃; for 2h;
DOI:10.1021/ja803012n

Reference yield:

: 1033588-19-0
C₆₂H₁₁₁NO₁₀SeSi₄

: 1033588-21-4
C₃₈H₅₅NO₁₀Se

Guidance literature:: With tris(dimethylamino)sulfonium trimethylsilyldifluoride; water; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 - 20 ℃; for 2h;
DOI:10.1021/jo3026077

Reference yield:

: C₂₉H₄₈O₅Si

: 1033588-21-4
C₃₈H₅₅NO₁₀Se

Guidance literature:: Multi-step reaction with 11 steps

1.1: water; sodium periodate / tetrahydrofuran; diethyl ether / 2 h / 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / 0.25 h / -78 °C / Inert atmosphere

2.2: -78 - -40 °C / Inert atmosphere

2.3: 0.5 h / -40 °C / Inert atmosphere

3.1: dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

4.1: water; acetic acid / tetrahydrofuran / 5 h / -20 °C

5.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 12 h / 20 °C / Inert atmosphere

5.2: 19 h / 20 °C / Inert atmosphere

6.1: methanol; barium hydroxide octahydrate / 0.33 h / 20 °C

7.1: tetrapropylammonium perruthennate / dichloromethane / 0.5 h / 20 °C

7.2: 24 h / 20 °C

8.1: (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; dimethylsulfide borane complex / tetrahydrofuran; dichloromethane; toluene / 0.75 h / -20 °C / Inert atmosphere

9.1: titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane; decane / 5 h / -20 °C / Molecular sieve; Inert atmosphere

10.1: tributylphosphine / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

11.1: tris(dimethylamino)sulfonium trimethylsilyldifluoride; water / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 0 - 20 °C

With titanium(IV) isopropylate; methanol; tert.-butylhydroperoxide; dmap; sodium periodate; tetrapropylammonium perruthennate; barium hydroxide octahydrate; tributylphosphine; dimethylsulfide borane complex; 2,4,6-trichlorobenzoyl chloride; tris(dimethylamino)sulfonium trimethylsilyldifluoride; water; acetic acid; triethylamine; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; decane; dichloromethane; N,N-dimethyl-formamide; toluene; 9.1: |Sharpless Asymmetric Epoxidation;
DOI:10.1021/jo3026077