C₃₁H₄₆O₅Si

Base Information

Chemical Name:C₃₁H₄₆O₅Si
CAS No.:1028432-87-2
Molecular Formula:C₃₁H₄₆O₅Si
Molecular Weight:526.789
Hs Code.:

C<sub>31</sub>H<sub>46</sub>O<sub>5</sub>Si

Synonyms:C₃₁H₄₆O₅Si

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Chemical Property of C₃₁H₄₆O₅Si

Chemical Property:

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Technology Process of C₃₁H₄₆O₅Si

There total 17 articles about C₃₁H₄₆O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1028432-64-5
C₄₅H₅₈O₅Si

: 1028432-87-2
C₃₁H₄₆O₅Si

Guidance literature:: With lithium 4,4′-di-tert-butylbiphenylide; In tetrahydrofuran; at -78 - -40 ℃; Inert atmosphere;
DOI:10.1021/ol800685c

Reference yield:

: 908865-92-9
(2S,3S)-6-(tert-Butyl-diphenyl-silanyloxy)-3-(4-methoxy-benzyloxy)-2-methyl-hexan-1-ol

: 1028432-87-2
C₃₁H₄₆O₅Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0.75 h / 20 °C

2.1: tert.-butyl lithium; 9-methoxy-9-BBN / tetrahydrofuran; diethyl ether; hexane; pentane / 1.17 h / -78 - 20 °C

2.2: 50 °C

3.1: 2,3-Dimethyl-2-butene; dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

3.2: 0 - 20 °C

4.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0 - 20 °C / Molecular sieve

5.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 0 °C / pH 7 / aq. phosphate buffer

6.1: zinc trifluoromethanesulfonate / dichloromethane / 12 h / 20 °C

7.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / -78 °C

7.2: -78 - 0 °C

8.1: 20% palladium hydroxide on charcoal; hydrogen / ethyl acetate / 20 °C

With 1H-imidazole; tetrapropylammonium perruthennate; 2,3-Dimethyl-2-butene; dimethylsulfide borane complex; 20% palladium hydroxide on charcoal; hydrogen; iodine; tert.-butyl lithium; zinc trifluoromethanesulfonate; 4-methylmorpholine N-oxide; 9-methoxy-9-BBN; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; ethyl acetate; pentane; 2.2: Suzuki-Miyaura coupling;
DOI:10.1002/chem.201101437

Reference yield:

: 1028432-61-2
C₅₂H₆₄O₆Si

: 1028432-87-2
C₃₁H₄₆O₅Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: 2,3-Dimethyl-2-butene; dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

1.2: 0 - 20 °C

2.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0 - 20 °C / Molecular sieve

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 0 °C / pH 7 / aq. phosphate buffer

4.1: zinc trifluoromethanesulfonate / dichloromethane / 12 h / 20 °C

5.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / -78 °C

5.2: -78 - 0 °C

6.1: 20% palladium hydroxide on charcoal; hydrogen / ethyl acetate / 20 °C

With tetrapropylammonium perruthennate; 2,3-Dimethyl-2-butene; dimethylsulfide borane complex; 20% palladium hydroxide on charcoal; hydrogen; zinc trifluoromethanesulfonate; 4-methylmorpholine N-oxide; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1002/chem.201101437