2-Bromo-3-methylfuran

Base Information

• Chemical Name: 2-Bromo-3-methylfuran
• CAS No.: 64230-60-0
• Molecular Formula: C₅H₅BrO
• Molecular Weight: 160.998
• Hs Code.: 2932190090
• DSSTox Substance ID: DTXSID00562198
• Nikkaji Number: J150.457F
• Wikidata: Q72447142

Synonyms:2-BROMO-3-METHYLFURAN;64230-60-0;Furan, 2-bromo-3-methyl-;2-bromo-3-methyl-furan;SCHEMBL7079516;DTXSID00562198;CS-0144563;F53471

Chemical Property of 2-Bromo-3-methylfuran

Chemical Property:

• Vapor Pressure: 10.389mmHg at 25°C
• Boiling Point: 133.51°C at 760 mmHg
• Flash Point: 34.546°C
• PSA: 13.14000
• Density: 1.538g/cm³
• LogP: 2.35050
• XLogP3: 2.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 159.95238
• Heavy Atom Count: 7
• Complexity: 65.1

Purity/Quality:

97% ^*data from raw suppliers

2-BROMO-3-METHYLFURAN 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(OC=C1)Br

Technology Process of 2-Bromo-3-methylfuran

There total 3 articles about 2-Bromo-3-methylfuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methylfuran (930-27-8) → 2-bromo-3-methylfuran (64230-60-0)

Guidance literature:

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In diethyl ether; for 1.5h; Heating;

DOI:10.1016/S0040-4020(01)86685-0

Reference yield:

3-methylfuran (930-27-8) + N-Bromosuccinimide (128-08-5) → 2-bromo-3-methylfuran (64230-60-0)

Guidance literature:

With (E)-3,3'-(diazene-1,2-diyl)bis(2-methylpropanenitrile); hydroquinone; calcium carbonate; In diethyl ether;

Reference yield:

→ 2-bromo-3-methylfuran (64230-60-0)

Guidance literature:

3-Methylfuran 4, NBS (1 Mol), Benzol, 2,2'-Azobisisobutyronitril, Δ, N2;

upstream raw materials:

3-methylfuran

N-Bromosuccinimide

Downstream raw materials:

longifolin

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